Preparation of Ag Nanoparticles by Particulate Radiation of Pulsed Electron Beam

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Nano metal Ag nanoparticles were synthesized by pulse electron beam (e-beam) irradiation at room temperature and the atmospheric pressure. The staring materials were AgNO3, toluene, ethanol and ethylene glycol. The ethanol and ethylene glycol plays a role of prohibiting agglomeration of metal ions. Energy dispersive X-ray spectrometer (EDX) was used to characterize the elements. Transmission electron microscopy (TEM) images were used to determine the shape and diameter. The time of e-beam irradiation affect to the particle size and aggregation. The average particle size was 10 nm and 30 nm for the dose time of 1 and 5 min, respectively. The shape of particles were changed from spherical to disk-like to coral-like, with increasing the irradiation time from 1 to 5 to 10 min.

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Advanced Materials Research (Volumes 287-290)

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338-342

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July 2011

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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[1] J. Shi, Z.Wang, H. L. Li, J. Nanopart Res. 8 (2006) 743.

Google Scholar

[2] K. Motesharei, D. C. Myles, J. Am Chem. 116 (1994) 7413.

Google Scholar

[3] S. Grzesiak, J. Belloni, J.-L. Marignier, Radiation Phys. & Chem. 77 (2008) 713.

Google Scholar

[4] C. S. Thaxton, C. A. Mirkin, Nat. Biotechnol. 23 (2005) 681

Google Scholar

[5] J. Turkevich, P. L. Stevens, J. Hiller, Discuss. Faraday Soc. 11 (1951) 55.

Google Scholar

[6] H. H. Huang, F. Q. Yan, Y. M. Kek, C. H. Chew, G. Q. Xu, W. Ji, P. H. Oh, S. H. Tang, Langmuir 13 (1997) 172.

Google Scholar

[7] M. Ohtaki, N. Toshima, Chem. Lett. 4 (1990) 489.

Google Scholar

[8] M. T. Reetz, W. Helbig, J. Am. Chem. Soc. 116 (1994) 7401.

Google Scholar

[9] M. Gutierrez, A. Henglein, J. Am. Phys. Chem. B 97 (1993) 11368.

Google Scholar

[10] M. Zhang, M. Mosatafavi, J. Am. Phys. Chem. B 101 (1997) 8443

Google Scholar

[11] Y. Mizukoshi, K. Okisu, Y. Meada, T. A. Yamamoto, R. Oshima, Y. Nagata, J. Am. Phys. Chem. B 101 (1997) 7033.

Google Scholar

[12] M. Mostafavi, M. O. Delcourt, G. Picq, Radiat. Phys. Chem. 41 (1993) 453.

Google Scholar

[13] K. J. Lawson, D. J. Stephenson, J. Materials Science, Letters, 10(12) (1991) 699.

Google Scholar

[14] Y. A. Kotov, S. Yu. Dokovnin, and M. E. Malezine, Trends in Food Sci. & Tech. 14 (2003) 4.

Google Scholar

[15] T. Li, H. G. Park, S.–H. Choi, Mater. Chem. & Phys.105 (2007) 325.

Google Scholar

[16] W. X. Chen, J. Y. Lee, Z. L. Liu, Chem. Commun. (2002) 2588.

Google Scholar

[17] M. S. Rahuveer, S. Agrawl, N. Bisop, G.zramamath, Chem. Mater. 18 (2006) 1390.

Google Scholar