Synthesis of Bis(2, 4-Dihydro-2H-3-(4-N-Maleimido) Phenyl -1, 3-Benzoxazine)Isopropane

Abstract:

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The novel bis(2, 4-dihydro-2H-3-(4-N-maleimido) phenyl-1, 3-benzoxazine)isopropane (BMIPBI) was synthesized from maleic anhydride, p-nitroaniline, formaldehyde and 2,2-bis(4-hydr -oxyphenyl)propane by a few steps reactions via the N-(4-nitrophenyl)maleimide(NPMI), N-(4-amin -ophenyl)maleimide(APMI),1,3,5-three(4-(maleimido)phenyl)-1,3,5-triazine(TMIPT)intermediate production. The chemical structures of BMIPBI were confirmed by 1H-NMR, FT-IR and EA. The results show that the production was the target object BMIPBI. The synthesized condition had been studied too. The BMIPBI was a loosened yellow solid and the yield of product was 58.8%.

Info:

Periodical:

Advanced Materials Research (Volumes 287-290)

Edited by:

Jinglong Bu, Pengcheng Wang, Liqun Ai, Xiaoming Sang, Yungang Li

Pages:

688-693

DOI:

10.4028/www.scientific.net/AMR.287-290.688

Citation:

G. Tao et al., "Synthesis of Bis(2, 4-Dihydro-2H-3-(4-N-Maleimido) Phenyl -1, 3-Benzoxazine)Isopropane", Advanced Materials Research, Vols. 287-290, pp. 688-693, 2011

Online since:

July 2011

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$35.00

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