Optimization of Simultaneous Distillation Extraction of the Black Pepper

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Abstract:

The aim of this work was to optimize a simultaneous distillation-extraction (SDE) procedure for the volatile compounds of black pepper (Piper Nigrum L.). Several variables that could potentially affect the extraction efficiency, namely, the liquid: solid ratio (volume per mass), soaking time and simultaneous distillation-extraction time have been optimized by means of response surface methodology (RSM). The optimum technology conditions have been attained by RSM as follows: the ratio of liquid to solid 25:1, simultaneous distillation-extraction time 3h and the soaking time 1.5h, under the optimum operating conditions, the extraction yield was 1.458%.

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Periodical:

Advanced Materials Research (Volumes 396-398)

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1454-1457

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Online since:

November 2011

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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