Developing the Crystalline Structures and Dielectric Properties of Excess Bi2O3-Added 0.95(Na0.5Bi0.5)TiO3-0.05BaTiO3 Ceramics

Ying Hsun Lin; Ping Shou Cheng; Yuan Tai Hsieh; Wen Cheng Tzou; Chia Ching Wu; Kuang Tao Wang; Chang Fu Yang

doi:10.4028/www.scientific.net/AMR.415-417.981

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Developing the Crystalline Structures and Dielectric Properties of Excess Bi₂O₃-Added 0.95(Na_0.5Bi_0.5)TiO₃-0.05BaTiO₃ Ceramics

Abstract:

0.95 (Na_0.5Bi_0.5)TiO₃-0.05 BaTiO₃ (NBT-BT3) compositions with excess x wt% Bi₂O₃ (NBT-BT3-x, with x=0, 1, 2, and 3) are sintered at 1200°C. When excess Bi₂O₃ is added, the NBT-BT3-1 ceramic displays the largest grain sizes, after which the grain sizes apparently decrease as more excess Bi₂O₃ is added. The lattice constants of calcined NBT-BT3 powder and NBT-BT3-x ceramics are calculated by the Rietveld full-pattern refinement method using the XRD standard pattern of ICSD-154041 and the measured XRD patterns of NBT-BT3-x ceramics. The refined values are compared with the measured XRD patterns to determine the cause of the distortion in the NBT-BT3-x ceramics. We show that NBT-BT3-1 ceramic has the minimum lattice constant a and maximum lattice constant c. The effects of excess Bi₂O₃ content on the dielectric properties of NBT-BT3-x ceramics are also discussed.