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A Novel Method for the Preparation of Nano-Sized Nickle Powders

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Abstract:

Nano-sized nickel powders were prepared through a wet chemical reduction, of NiCl2 by sodium in liquid ammonia at -45 °C, and a subsequent heat-treatment in vacuum at 300 °C. The prepared product was systematically characterized by X-ray diffraction (XRD), scan electron microscopy (SEM), transmission electron microscopy (TEM), and BET specific surface area measurement. The results show that the product was composed of nano-sized nickel particles, with average particle diameter of about 20 nm, and specific surface area of about 30 m2g-1. The possible formation mechanism of the nano-sized nickel powder was also discussed briefly.

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Periodical:

Advanced Materials Research (Volumes 512-515)

Pages:

1849-1853

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.512-515.1849

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Online since:

May 2012

Authors:

Zhao Han, Hong Min Zhu

Keywords:

Heat Treatment, Nanocrystalline Powders, Nickel, Reduction

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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