Effects of Reductant Amount and Capping Agent on Tin Nanoparticles Synthesis Using a Tin(II) 2-Ethylhexanoate Precursor

Sang Soo Chee; Jong Hyun Lee

doi:10.4028/www.scientific.net/AMR.530.52

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 530Effects of Reductant Amount and Capping Agent on...

Effects of Reductant Amount and Capping Agent on Tin Nanoparticles Synthesis Using a Tin(II) 2-Ethylhexanoate Precursor

Abstract:

Tin nanoparticles were synthesized through compulsive reduction using a Tin(II) 2-ethylhexanoate precursor, and the effect of reductant (sodium borohydride) amount on the size distribution of the particles was surveyed. Issues caused by the absence of a capping agent (polyvinyl pyrrolidone) were similarly examined. An excessive amount of dissolved sodium borohydride caused variations in the tin nanoparticle sizes, from a few nanometers to several tens of nanometers. The formation of abnormally large particles was attributed to the vigorous coagulation among smaller tin particles. In the tin nanoparticles synthesized without polyvinyl pyrrolidone, an exceptionally wide size distribution was observed owing to irregularly coagulated and aggregated large particles.

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Periodical:

Advanced Materials Research (Volume 530)

Pages:

52-55

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.530.52

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Online since:

June 2012

Authors:

Sang Soo Chee, Jong Hyun Lee

Keywords:

Capping Agent, Reductant, Reduction Synthesis, TiN Nanoparticles, Tin(II) 2-Ethylhexanoate

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