Effect of Annealing on the Magnetostatic and Microwave Electromagnetic Properties of Glass-Coated Fe-Rich Microwires

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Abstract:

Glass-coated FeCuNbVSiB microwires was annealed in the temperature range of 380 °C to 600 °C. The microstructures and magnetostatic properties of the glass-coated microwires were characterized by X–ray diffraction (XRD), Vibrating Sample Magnetometer (VSM) respectively. Relative complex permeability and complex permittivity was measured by transmission/reflection (T/R) coaxial line method in the frequency range of 2-18 GHz for as-casted and annealed Fe-rich microwires samples. The measured results show that the coercive field of the Fe-rich microwires decrease to 1.54 Oe at 470 °C, and then increase rapidly with the increasing of the annealing temperature. The coercive field and saturation field of the microwire samples increased abruptly with the outgrowth of the Fe-B hard magnetic phase in the Fe-rich microwire samples. The imaginary part of permeability and the natural ferromagnetic resonance frequency decrease for the thermal treatment below 470 °C, and then increase with the annealing temperature up to 530 °C. The change of magnetostatic and microwave electromagnetic properties of the microwires samples with the annealing process come from the change of the anisotropy caused by the internal stress.

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Advanced Materials Research (Volumes 562-564)

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345-349

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August 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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