Synthesis of Silica Microspheres Filler for PDMS

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A new kind of silica microspheres were first synthesized with chloropropyltrimethoxysilane (WD30) and tetraethoxysilane (TEOS) by sol-gel method. And hybrid membrane was prepared by incorporating the as prepared filler into polydimethylsiloxane (PDMS). The IR, swelling density(Dsw) and mechanical properties of these composites membranes were studied by means of IR analysis and tensile testing. The experimental results showed that both mechanical properties of these composites were significantly improved by using the as-synthesized filler. The filler synthesized in this research not only increased the volume and reduce the cost of HPDMS, but also reacted with the PDMS. The vulcanztion density was increasedwith the interaction between the filler and the PDMS chains. This new kind of silica microspheres is an effective reinforcement filler for PDMS composite.

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190-193

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January 2013

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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