Analysis of Extraction of Coal Oxidation Residue in NaOCl

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Abstract:

Sequential extraction of four coal oxidation residues (COR) from aqueous NaOCl solution with petroleum ether (PE), carbon disulfide (CS2), acetone and methanol were investigated. The results suggest that methanol is an effective extraction solvent, giving the highest extraction yields for four COR. The extraction fractions were analyzed by GC/MS. It is found that no compounds, except for F1 of HL and XL , F2 of four COR, were detected. In total, 89 organic compounds were detected in F1 of HL and XL, 23 organic compounds in F2 from four COR. Most of which were arenes (As), normal alkanes (NAs) and oxygen-containing compounds (OCCs).

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Advanced Materials Research (Volumes 724-725)

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1103-1106

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August 2013

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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[1] K. Miura, K. Mae, H. Okutsu and N. Mizutani: Energy Fuels vol. 10 (1996), pp.1196-1201.

Google Scholar

[2] K. Mae, H. Shindo and K. Miura: Energy Fuels vol. 15 (2001), pp.611-617.

Google Scholar

[3] Z.X. Liu, Z. C. Liu, Z.M. Zong, X. Y. Wei, J. Wang and C. W. Lee: Energy Fuels vol. 17 (2003), pp.424-426.

Google Scholar

[4] S. R. Palmer, E. J. Hippo and X. A. Dorai: Fuel vol. 73 (1994), pp.161-169.

Google Scholar

[5] E. H. Cho and Q. Luo: Fuel Process. Technol. vol. 46 (1996), pp.25-39.

Google Scholar

[6] Y. G. Huang, Z. M . Zong, Z. S. Yao, Y. X. Zheng, J. Mou, G. F. Liu, J. P. Cao, M. J. Ding, K. Y. Cai, F. Wang, W. Zhao, Z. L. Xia and X. Y. Wei: Energy Fuels vol. 22 (2008), pp.1799-1806.

DOI: 10.1021/ef700589q

Google Scholar

[7] S. Murata, Y. Tani, M. Hiro, K. Kidena, L. Artok, M. Nomura and M. Miyake: Fuel vol. 80 (2001), pp.2099-2109.

DOI: 10.1016/s0016-2361(01)00093-x

Google Scholar

[8] Z. S. Yao, X. Y. Wei, J. Lv, F. J. Liu, Y. G. Huang, J. J. Xu, F. J. Chen, Y. Huang, Y. Li, Y. Lu and Z. M. Zong: Energy Fuels vol. 24 (2010), pp.1801-1808.

DOI: 10.1021/ef9012505

Google Scholar

[9] G. Z. Gong, X. Y. Wei and Z. M. Zong: J Fuel Chem Technol vol. 40 (2012), pp.1-7.

Google Scholar

[10] P. A. Peng, J. Fu, G. Sheng, A. Morales-Izquierdo, E. M. Lown and O. P. Strausz: Energy Fuels vol. 13 (1999), pp.266-277.

DOI: 10.1021/ef980235k

Google Scholar

[11] J. S. Do and T. C. Chou: J. Appl. Electrochem. vol. 19 (1989), pp.922-927.

Google Scholar