Catalytic Synthesis of Isoamyl Acetate by Ion Exchange Resin-Supported (NH4)6[MnMo9O32] • 8H2O with Waugh Structure

Li Xia Wang; Shu Heng Liu; Hua Yuan; Lin Lin Guo

doi:10.4028/www.scientific.net/AMR.750-752.1231

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 750-752Catalytic Synthesis of Isoamyl Acetate by Ion...

Catalytic Synthesis of Isoamyl Acetate by Ion Exchange Resin-Supported (NH₄)₆[MnMo₉O₃₂] • 8H₂O with Waugh Structure

Abstract:

Ion exchange resin-supported (NH₄)₆[MnMo₉O₃₂]8H₂O with Waugh structure is used to prepare supported solid catalyst. Performance of this catalyst is researched by means of synthesis of isoamyl acetate. Optimal reaction conditions determined by orthogonal experiment are as follows: acid-alcohol molar ratio is 2.5:1, reaction time is 120 min, catalyst dosage is 0.8 g, dosage of water-carrying agent is 2.5 ml, esterification yield reaches 95.1%. This catalyst is characterized by high catalytic efficiency, easy separation and recovery, absence of environmental pollution and being reusable, etc.

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Periodical:

Advanced Materials Research (Volumes 750-752)

Pages:

1231-1234

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.750-752.1231

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Online since:

August 2013

Authors:

Li Xia Wang*, Shu Heng Liu, Hua Yuan, Lin Lin Guo

Keywords:

Catalyst, Ion Exchange Resin-Supported, Isoamyl Acetate, Waugh Structure

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