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Research on the Synthetic of Silicone Emulsion
Abstract:
This study synthesized silicon emulsions by emulsion polymerization, mainly focused on how influencing factors including catalyst, emulsifier, reaction temperature and synthesis process could affect product conversion rate, appearance and molecular weight. The result showed that the conversion rate of the first 2 hours increased rapidly and became stable afterwards. Molecular weight increment was proportional to the extension of the reaction time. The silicon emulsions could achieve high convention rate and stability while applying 5% catalyst DBSA and 3% emulsifier (OP-10: SDS = 1:2) of Octmethyl cyclotetrasiloxane(D4) under an reaction temperature of 80 °C.
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233-236
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November 2013
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© 2013 Trans Tech Publications Ltd. All Rights Reserved
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