MgO Nanostructured Materials Obtained Via the Solid-State Reaction Method

Nor Fadilah Chayed; Norlida Kamarulzaman; Nurhanna Badar; Rusdi Roshidah; Norashikin Kamarudin; Mohd Sufri Mastuli

doi:10.4028/www.scientific.net/AMR.895.347

Paper Titles

Spectroscopic Studies of Er³⁺-Yb³⁺ Codoped Multicomposition Tellurite Oxide Glass
p.323

Electrochemical Behavior of LiCo_(1-x)Mn_xO₂ Crystalline Powders
p.334

Effect of Two Annealing Temperatures on the Phases of Novel σ-Al_1.9Zn_0.1O₃ Nanopowders
p.338

Investigation of Phase, Purity, Morphology and Particle Size of Zn_(1-x)Cu_xO Materials via X-Ray Diffraction (XRD) and Microscopic Techniques
p.343

MgO Nanostructured Materials Obtained Via the Solid-State Reaction Method
p.347

Effect of Calcination Time on the Specific Capacities of LiNi_0.4Co_0.55Ti_0.05O₂ Cathode Materials
p.351

The Effect of Fe and Al Substitution in LiNi_0.8Co_0.2O₂Cathode Material
p.355

The Influence of Yb³⁺ Co-Doping on Optical Properties of Sm³⁺-Doped Sodium Tellurite Glasses
p.359

Preparation and Characterization of Soft Glass Using Sarawak Silica Sand as Starting Material for Craftware
p.363

HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 895MgO Nanostructured Materials Obtained Via the...

MgO Nanostructured Materials Obtained Via the Solid-State Reaction Method

Abstract:

Recently, several synthesis methods have been reported for producing magnesium oxide (MgO) nanostructures such as sol-gel, combustion, thermal evaporation, chemical precipitation, etc. This work describes a simple method to synthesize MgO nanostructures via a conventional solid-state reaction method using magnesium acetate tetrahydrate as a starting material. Magnesium acetate tetrahydrate was directly annealed at a temperature of 600 °C and 800 °C for 24 h. The X-Ray Diffraction (XRD) revealed that the annealed samples were pure while Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM) showed different morphologies of MgO. From the results, it is found that TEM may reveal information that cannot be observed in the SEM micrographs.

You might also be interested in these eBooks

View Preview

Info:

Periodical:

Advanced Materials Research (Volume 895)

Pages:

347-350

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.895.347

Citation:

Cite this paper

Online since:

February 2014

Authors:

Nor Fadilah Chayed*, Norlida Kamarulzaman, Nurhanna Badar, Rusdi Roshidah, Norashikin Kamarudin, Mohd Sufri Mastuli

Keywords:

MgO, Solid-State Reaction

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

* - Corresponding Author

References

[1] M. A. Shah, A. Qurashi, Journal of Alloys and Compounds Vol. 482, pp.548-551.

Google Scholar

[2] K. H. Nam and J. G. Han: Surface and Coatings Technology Vol. 171, pp.51-58.

Google Scholar

[3] X. Fu, Z. Song, G. Wu, J. Huang, X. Duo and C. Lin: Journal of Sol-Gel Science and Technology Vol. 6, pp.277-281.

Google Scholar

[4] L. Kumari, W. Z. Li, C. H. Vannoy, R. M. Leblanc and D. Z. Wang: Ceramics International Vol. 35, pp.3355-3364.

Google Scholar

[5] H. Lu, L. Liao, H. Li, Y. Tian, D. F. Wang, J. C. Li, B. P. Zhu and Y. Wu: Solid State Communications Vol. 147, pp.57-60.

Google Scholar

[6] A. Kumar and J. Kumar: Journal of Physics and Chemistry of Solids Vol. 69, pp.2674-2772.

Google Scholar

[7] Z. Cui, G. W. Meng, W. D. Huang, G. Z. Wang and L. D. Zhang: Materials Research Bulletin Vol. 35, pp.1653-1659.

Google Scholar

[8] W. Wang, X. Qiao, J. Chen and H. Li: Materials Letters Vol. 61, pp.3218-3220.

Google Scholar

[9] K. P. Kalyanikutty, F. L. Deepak, C. Edem, A. Govindaraj and C.N.R. Rao: Materials Research Bulletin Vol. 40, pp.831-839.

DOI: 10.1016/j.materresbull.2005.01.013

Google Scholar