Ultrasonic Synthesis of Ag2Se Nanocrystal in Perrhenate Solution

Wei Jun Shan; Qiang Yan; Du Li; Da Wei Fang; Shu Liang Zang

doi:10.4028/www.scientific.net/AMR.919-921.2109

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 919-921Ultrasonic Synthesis of Ag2Se Nanocrystal in...

Ultrasonic Synthesis of Ag₂Se Nanocrystal in Perrhenate Solution

Abstract:

Ag₂Se nanocrystal was successfully prepared by ultrasonic synthesis in water and ethanol systems at an ambient pressure. The powder of selenium was used as the selenium ion source. The size of the nanocrystals is in the scope of 10-20nm. The products were characterized by some means including X-ray Powder Diffraction (XRD) and Transmission Electron Microscopy (TEM) which was used to study the thermostability of the product. The result of the experiments indicated that the concentration of the reactant, the pH of the solution, the react temperature and the surfactant had some important influence on the formation and the size of the Ag₂Se nanoparticles. The method we reported here is proved to be a new and an easy way to prepare the nanocrystals of metal chalcogenide.

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Periodical:

Advanced Materials Research (Volumes 919-921)

Pages:

2109-2111

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.919-921.2109

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Online since:

April 2014

Authors:

Wei Jun Shan, Qiang Yan, Du Li, Da Wei Fang*, Shu Liang Zang

Keywords:

Ag₂Se, Nanocrystal, Precipitation, Ultrasonic Synthesis

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References

[1] Y L Yan, X F Qian, H J Xu, J Yin, Z K Zhu, A novel solid-liquid route for the preparation of Cu3Se2 and Ag2Se nano crystals, INORGANIC CHEMISTRY COMMUNICATIONS 6 (2003) 34-37.

DOI: 10.1016/s1387-7003(02)00673-1

Google Scholar

[2] H L Su, Y Xie, B Li, Y T Qian, Simple, convenient, mild hydrothermal route to nano crystalline CuSe and Ag2Se, MATERIALS RESEARCH BULLETIN 35 ( 2000) 465-469.

DOI: 10.1016/s0025-5408(00)00233-6

Google Scholar

[3] M V Busch, T G Van, P Monnoyer, J B Nagy, Structural characterization of colloidal Ag2Se nano crystals LANGMUIR 14 (1998) 1528-1531.

Google Scholar

[4] R Z Chen, D S Xu, G L Guo, L L Gui, Silver selenide nano-wires by electro-deposition JOURNAL OF THE ELECTROCHEMICAL SOCIETY 150 (2003)183-186.

Google Scholar

[5] Y J Glanville, D G Narehood, P E Sokol, A Amma, T Mallouk Preparation and synthesis of Ag2Se nano wires produced by template directed synthesis, JOURNAL OF MATERIALS CHEMISTRY, 12 (2002) 2433-2434.

DOI: 10.1039/b202913h

Google Scholar

[6] Y Jiang, B Xie, J Wu, S W Yuan, Y Wu, H Huang, Y T Qian, Room-temperature synthesis of copper and silver, nano crystalline chalcogenides in mixed solvents, JOURNAL OF SOLID STATE CHEMISTRY 167 (2002) 28-33.

DOI: 10.1006/jssc.2002.9610

Google Scholar