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Effect of Calcination Temperature on the Morphology of Carbon Nanosphere Synthesized from Polymethylmethacrylate

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Abstract:

In this work, hollow carbon nanospheres (HCNs) were synthesized by carbonizing core/shell particles of polymethylmethacrylate (PMMA)/ resorcinol formaldehyde. The core/shell particles were prepared using emulsion polymerization; polymethylmethacrylate as a template and resorcinol-formaldehyde polymer as the carbon source. Spheres were first synthesized by batch mode polymerization and then the shell was polymerized on the surface of the spheres. The composite was stabilized, and then carbonized. The effect of calcination temperature was investigated in the range between 200-500 oC. Scanning electron microscopy (SEM), energy-dispersive X-ray spectrometer (EDX), Raman and Fourier transform infrared (FTIR) were used for characterization of the resulting carbon.

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Periodical:

Advanced Materials Research (Volume 974)

Pages:

55-59

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.974.55

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Online since:

June 2014

Authors:

Abdullah F. Al-Ahmadi*, Mohammed A. Al-Daous, Tawfik A. Saleh

Keywords:

Carbon Nanosphere, Morpholoy, Poly(methyl methacrylate) (PMMA), Temperature

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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References

[1] A.H. Lu, G.P. Hao, Q. Sun, X.Q. Zhang and W.C. Li, Macromol. Chem. Phys. 213 (2012) 1107−1131.

Google Scholar

[2] A.A. Deshmukh, S.D. Mhlanga and N.J. Coville, Carbon spheres, Materials Scie. Eng. R 70 (2010) 1–28.

Google Scholar

[3] A.C. Ferrari and J. Robertson, Physical Review b 61, 20 (2000) 15.

Google Scholar

[4] Y. Mi ,W. Hu , Y. Dan and Y. Liu, Materials Letters 62 (2008) 1194–1196.

Google Scholar

[5] L. Zubizarreta, J.A. Menendez, J.J. Pis and A. Arenillas, Int. Hydrogen Energy, 34 (2009) 3070–3076.

Google Scholar

[6] A.N. Marquez, R. Romero, A. Romeroa and J.L. Valverde, J. Mater. Chem., 21 (2011) 1664–1672.

Google Scholar

[7] M. Peer, A. Qajar and R. Rajagopalan, H.C. Foley, Carbon 51 (2013)85-93.

Google Scholar

[8] J. Ryu, Y.W. Suh, D.J. Suh and D.J. Ahn, Carbon 48 (2010) 1990 –(1998).

Google Scholar

[9] M.M. Titirici and Markus Antonietti, Chem. Soc. Rev., 2010, 39, 103–116.

Google Scholar

[10] L. Zhao, N. Baccile, S. Gross, M. Antonietti and M. M. Titirici, Carbon, 48 (2010) 378-382.

Google Scholar

[11] S.H. Joo, et al. Nature 412 (2001) 169–172.

Google Scholar

[12] Z.Y. Wang, F. Li and A. Stein, Nano Lett. 7 (2007) 3223–3326.

Google Scholar

[13] J.L. Gu, S.S. Su, Y.S. Li, Q. He and J.L. Shi, Chem. Commun. 47 (2011) 2101–2103.

Google Scholar

[14] D. Gu, et al., Adv. Mater. 22 (2010) 833–837.

Google Scholar

[15] Y. Fang, et al., Angew. Chem. Int. Ed. 49 (2010) 7987–7991.

Google Scholar

[16] J. Liu, et al. Nat. Commun. 4: 2798 doi: 10. 1038/ncomms3798 (2013).

Google Scholar

[17] D. Wu, R. Fu and Z. Yu, J Appl Polym Sci; 96 (2005) 1429–35.

Google Scholar

[18] K. Nakanishi and P.H. Solomon. Infrared adsorption spectro. 2nd ed. San Franc: Holden-Day; 1977. p.19–21.

Google Scholar

[19] N. Baccile, G. Laurent, F. Babonneau, F. Fayon, M.M. Titirici, M. Antonietti, J. Phys. Chem C; 113(2009) 9644–54.

DOI: 10.1021/jp901582x

Google Scholar

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