Preparation of PLZT Powders from Oxides via High-Energy Ball Milling Process

Qing Song Peng; Wan Jiang; Jing Feng Li

doi:10.4028/www.scientific.net/KEM.280-283.623

Paper Titles

Study on the Synthetic Process of Calcium Borate
p.605

Synthesis of BiFeO₃-PbTiO₃ Powders by Sol-Gel Auto-Combustion Process
p.609

Process for Non-Agglomerated Nanometer-Sized Barium Titanate Powders by Sol-Gel Auto-Igniting Synthesis
p.613

Preparation and Characterization of BaTiO₃ Powders by Sol-Gel and BaTiO₃ Ferroelectric Films by Electrophoretic Deposition Technique
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Preparation of PLZT Powders from Oxides via High-Energy Ball Milling Process
p.623

Synthesis of Perovskite Pb(Zr_0.52Ti_0.48)O₃ (PZT) Powders by a Modified Coprecipitation Method
p.627

Preparation of Nanocrystalline Ba₃(Ca_1.18Nb_1.82)O_9-δ Powder with Sol-Gel Auto-Ignition Synthesis Process
p.631

Low-Temperature Synthesis of PMnN-PZT Powders by Hybrid Method of Sol-Gel and Ultrasonic Atomization
p.635

Characteristics of Sr₂CeO₄ Powder Phosphor Prepared by Combustion Route
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Preparation of PLZT Powders from Oxides via High-Energy Ball Milling Process

Abstract:

Lanthanum-modified lead zirconate-titanate (PLZT5/54/46) powders were prepared from the commercial PbO, La2O3, TiO2 and ZrO2 powders by high-energy ball milling process. The synthesized powders milled for different hours were characterized using XRD and SEM. Thedesigned PLZT perovskite phase was formed from the mixture of the starting materials after milling for 20 hours. PLZT(5/54/46) ceramics were obtained using the produced powders milled for 20 h followed by sintering at temperatures ranging from 1000 to1200°C. Ferroelectric property of the PLZT ceramics was also measured.