TEM Study of SiCN Glasses; Polymer Architecture versus Ceramic Microstructure

Article Preview

Abstract:

Polymer-derived SiCN glasses with tailored polymer architectures were characterized by TEM and EF-SAED upon pyrolysis at 1000 °C and subsequent annealing. Main emphasis of this work was to verify as to whether the intrinsic amorphous structure of polymer-derived bulk materials exhibits different structural features upon pyrolysis, depending on the functionalities of the pre-ceramic polymer, and whether such characteristic features are maintained upon high-temperature anneal.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

153-156

Citation:

Online since:

December 2008

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2009 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] W. Verbeek, and G. Winter, (in Ger. ) Ger. Pat. No. 2236078, (1974).

Google Scholar

[2] S. Yajima, K. Okamura, J. Hayashi and M. Omori, J. Am. Ceram. Soc., 59 [7-8] (1976), p.324.

Google Scholar

[3] G. Yu, M. J. Ediringshe, D.S. Finch, B. Ralph and J. Parrick, J. Eur. Ceram. Soc., 15 (1995), p.581.

Google Scholar

[4] T. Vaahs, M. Brück and W.D.G. Böcker, Adv. Mater., 4.

Google Scholar

[3] (1992), p.224.

Google Scholar

[5] J. Bill and D. Heimann, J. Eur. Ceram. Soc. 16, (1996), p.1115.

Google Scholar

[6] M.R. Mucalo, N.B. Milestone, I.C. Vickridge and M.V. Swain, J. Mater Sci., 29 (1994), p.4487.

Google Scholar

[7] H. -J. Kleebe, D. Suttor, H. Müller and G. Ziegler: J. Am Ceram. Soc., 81.

Google Scholar

[11] (1998), p.2971.

Google Scholar

[8] H. -J. Kleebe, H. Störmer, S. Trassl and G. Ziegler: Appl. Organomet. Chem., 15 (2001), p.858.

Google Scholar

[9] M. Monthioux and O. Delverdier: J. Eur. Ceram. Soc., 16 (1996), p.721.

Google Scholar

[10] J. Bill and F. Aldinger: Adv. Mater., 7.

Google Scholar

[9] (1995), p.775.

Google Scholar

[11] J. Bill et al.: Appl. Organometal. Chem., 15 (2001), p.777.

Google Scholar

[12] J. Lücke, J. Hacker, D. Suttor and G. Ziegler: Appl. Organometal. Chem., 11 (1997), p.184.

Google Scholar

[13] G. Motz, J. Hacker and G. Ziegler: in Ceramic Engineering & Science Proceeding, Vol. 21. Edited by. T. Jessen and E. Ustundag, Cocoa Beach, Florida, 2000, p.307.

Google Scholar

[14] S. Traßl, D. Suttor, G. Motz E. Rössler and G. Ziegler: J. Eur. Ceram Soc., 20 (2000), p.215.

Google Scholar

[15] S. Traßl, G. Motz E. Rössler and G. Ziegler: J. Am. Ceram Soc., 85.

Google Scholar

[1] (2002), p.239.

Google Scholar