Effects of Sintering Temperature on Structural and Electrical Transport Properties of Zinc Ferrites Prepared by Sol-Gel Route

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Abstract:

The effects of sintering temperature on the structural and electrical transport properties of nanocrystalline zinc ferrites are reported. The zinc ferrites were prepared by WOWS sol-gel synthesis route. The prepared sample was sintered at temperatures 500°C, 700°C and 900°C respectively for 2 h. X-ray Diffraction (XRD) technique was used to describe the structural properties. The crystallite size, lattice parameters and porosity of samples were measured from the analysis of XRD data. The average crystallite size for each sample was measured using the Scherrer formula by considering the most intense (3 1 1) peak. The dielectric constant (ε), dielectric loss tangent (tan ) and AC electrical conductivity of nanocrystalline Zn ferrites are investigated as a function of frequency and sintering temperature. All the electrical properties are explained in accordance with MaxwellWagner model and Koops phenomenological theory.

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Key Engineering Materials (Volumes 510-511)

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585-590

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May 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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