High Quality Al2O3 Nanoparticles Used for Energy Saving Lamps

Article Preview

Abstract:

High quality Al2O3 nanoparticles have been successfully synthesized by a simple sol-gel method. Analysis on phase and structure based on x-ray diffraction (XRD) techniques indicate that the as-synthesized samples are well crystallized γ-Al2O3. High-resolution transmission electron microscopy (HRTEM) techniques further confirm a NP is single crystal with size less than 20 nm, the size distribution is uniform as a whole. Raman spectra analysis indicates the vibrational models are in accordance with γ-Al2O3. The density of the obtained γ-Al2O3 nanoparticles material is very small and have a loosen structure, elemental analysis suggests that the nanoparticles are high purity. The as-synthesized γ-Al2O3 material is comparable to the corresponding products that bought abroad in structure, density and purity, and is suitable for energy saving lamps.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

228-231

Citation:

Online since:

July 2012

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2012 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] J.H. Yi, Y.Y. Sun, J.F. Gao, C.Y. Xu, Synthesis of Crystalline g-Al2O3 with high purity, Trans. Nanoferrs. Met. Soc. China 19 (2009) 1237-1242.

Google Scholar

[2] M. Shojaie-Bahaabad, E. Taheri-Nassaj, Economical synthesis of nano alumina powder using an aqueous sol–gel method, Materials Letters, 62 (2008) 3364−3366.

DOI: 10.1016/j.matlet.2008.03.012

Google Scholar

[3] C. Franklin, A. Daniel, F.G. Osvaldo, Dehydrogenation of propane on chromia/alumina catalysts promoted by tin, Catalysis Today, 133/135 (2008) 800−804.

DOI: 10.1016/j.cattod.2007.12.039

Google Scholar

[4] J.M. McHale, A. Auroux, J.M. Perrotta, A. Navrotsky, Surface Energies and Thermodynamic Phase Stability in Nanocrystalline Aluminas, Science 277 (1997) 788-791

DOI: 10.1126/science.277.5327.788

Google Scholar

[5] D.J. Suh, T.J. Park, J.H. Kim, K.L. Kim, Preparation and Catalytic Applications of High-Surface-Area Aerogels, Chem. Mater. 9 (1997) 1903-1905.

Google Scholar

[6] T. Johannessen, S.E. Pratsinis, H. Livbjerg, Computational fluid-particle dynamics for the flame synthesis of alumina particles, Chem. Eng. Sci. 55 (2000) 177-188.

DOI: 10.1016/s0009-2509(99)00183-9

Google Scholar

[7] W.Q. Cai, H.Q. Li, Y. Zhang. Azeotropic distillation-assisted preparation of macro- mesostructured g-Al2O3 nanofibres of crumpled sheet-like morphology, Mater. Chem. Phys. 96 (2006) 136−139.

DOI: 10.1016/j.matchemphys.2005.06.053

Google Scholar

[8] P.G. Li, M. Lei, W.H. Tang, Raman and photoluminescence properties of alpha-Al2O3 microphones with hierarchical and repetitive superstructure Materials Letters 64 (2010) 161–163.

DOI: 10.1016/j.matlet.2009.10.032

Google Scholar

[9] K. R. Nagabhushana, B. N. Lakahminarasappa, F. Singh, Photoluminescence and Raman studies in swift heavy ion irradiated polycrystalline aluminum oxide, Bull. Mater. Sci. 32 (2009) 515–519.

DOI: 10.1007/s12034-009-0076-y

Google Scholar

[10] J.J. Kingsley, K.C. Pail, A novel combustion process for the synthesis of fine particles of a-Al2O3 and related particles, Mater. Lett. 6 (1988) 427-432.

Google Scholar