Studying SiC/SiC Composites by X-Ray Tomography

Article Preview

Abstract:

Continuous SiC fiber reinforced SiC matrix composites (SiC/SiC) have been studied and developed for high temperature applications and nuclear applications. In this study, SiC/SiC composites were fabricated via polymer impregnation and pyrolysis (PIP) process and studied by X-ray tomography. The SiC/SiC composites were first scanned using a Metris X-tek 320 kV source at the Henry Moseley X-ray Imaging Facility at the University of Manchester, the closed porosities were investigated after three dimensional (3D) imaging of the samples. Furthermore, high-resolution synchrotron X-ray tomography was applied to the SiC/SiC composite at Diamond Light Source. Digital volume correlation was employed for Hertzian indentation testing of the SiC/SiC composite, quantifying damage by measurement of the displacement fields within the material. A Cellular Automata integrated with Finite Elements (CAFE) method was developed to account for the effect of microstructure on the fracture behavior of the SiC/SiC composite. Graded microstructures, textures and multiple phases were simulated and a mesh-free framework was developed to compute the damage development through the microstructure. The results indicated that we could study the development of discontinuous cracking and damage coalescence, and its sensitivity to microstructure with this method.

You might also be interested in these eBooks

Info:

Periodical:

Key Engineering Materials (Volumes 602-603)

Pages:

416-421

Citation:

Online since:

March 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] H. Ohnabe, S. Masaki, M. Onozuka, K. Miyahara, T. Sasa, Potential application of ceramic matrix composites to aero-engine components, Compos. Part A 30 (1999) 489-496.

DOI: 10.1016/s1359-835x(98)00139-0

Google Scholar

[2] J. Kimmel, N. Miriyala, J. Price, K. More, P. Tortorelli, H. Eaton, G. Linsey, E. Sun, Evaluation of CFCC liners with EBC after field testing in a gas turbine, J. Eur. Ceram. Soc. 22 (2002) 2769-2775.

DOI: 10.1016/s0955-2219(02)00142-5

Google Scholar

[3] R. Naslain, Design, preparation and properties of non-oxide CMCs for application in engines and nuclear reactors: an overview, Compos. Sci. Technol. 64 (2004) 155-170.

DOI: 10.1016/s0266-3538(03)00230-6

Google Scholar

[4] Y. Katoh, L. L. Snead, C. H. Henager, A. Hasegawa, A. Kohyama, B. Riccardi, H. Hegeman, Current status and critical issues for development of SiC composites for fusion applications, J. Nucl. Mater. 367-370 (2007) 659-671.

DOI: 10.1016/j.jnucmat.2007.03.032

Google Scholar

[5] L. L. Snead, T. Nozawa, M. Ferraris, Y. Katoh, R. Shinavski, M. Sawan, Silicon carbide composites as fusion power reactor structural materials, J. Nucl. Mater. 417 (2011) 330-339.

DOI: 10.1016/j.jnucmat.2011.03.005

Google Scholar

[6] B. Riccardi, L. Giancarli, A. Hasegawa, Y. Katoh, A. Kohyama, R. H. Jones, L. L. Snead, Issues and advances in SiCf/SiC composites development for fusion reactors, J. Nucl. Mater. 329 (2004) 56-65.

DOI: 10.1016/j.jnucmat.2004.04.002

Google Scholar

[7] T. Nozawa, T. Hinoki, A. Hasegawa, A. Kohyama, Y. Katoh, L. L. Snead, C. H. Henager, J. B. J. Hegeman, Recent advances and issues in development of silicon carbide composites for fusion applications, J. Nucl. Mater. 386-88 (2009) 622-627.

DOI: 10.1016/j.jnucmat.2008.12.305

Google Scholar

[8] A. Iveković, S. Novak, G. Dražić, D. Blagoeva, S. G. de Vicente, Current status and prospects of SiCf/SiC for fusion structural applications, J. Eur. Ceram. Soc. 33 (2013) 1577-1589.

DOI: 10.1016/j.jeurceramsoc.2013.02.013

Google Scholar

[9] E. N. Landis, D. T. Keane, X-ray microtomography, Mater. Charact. 61 (2010) 1305-1316.

Google Scholar

[10] A. Morales-Rodríguez, P. Reynaud, G. Fantozzi, J. Adrien, E. Maire, Porosity analysis of long-fiber- reinforced ceramic matrix composites using X-ray tomography, Scripta Mater. 60 (2009) 388-390.

DOI: 10.1016/j.scriptamat.2008.11.018

Google Scholar

[11] J. Ramirez-Rico, F. Stolzenburg, J. D. Almer, J. L. Routbort, D. Singh, K. T. Faber, In situ imaging and strain determination during fracture in a SiC/SiC ceramic matrix composite, Scripta Mater. 69 (2013) 497-500.

DOI: 10.1016/j.scriptamat.2013.05.032

Google Scholar

[12] C. Chateau, L. Gélébart, M. Bornert, J. Crépin, E. Boller, C. Sauder, W. Ludwig, In situ X-ray microtomography characterization of damage in SiCf/SiC minicomposites, Compos. Sci. Technol. 71 (2011) 916-924.

DOI: 10.1016/j.compscitech.2011.02.008

Google Scholar

[13] D. Wang, X. Mao, Y. Song, Y. Wang, Preparation and Properties of SiC Fiber with a Stable Excess Carbon Layer on the Surface, J. Inorg. Mater. 24 (2009) 1209-1213.

DOI: 10.3724/sp.j.1077.2009.01209

Google Scholar

[14] D. Zhao, H. Wang, X. Li, Development of Polymer-Derived SiC Fiber, J. Inorg. Mater. 24 (2009) 1097-1104.

Google Scholar

[15] H. Liu, H. Cheng, J. Wang, G. Tang, Effects of the single layer CVD SiC interphases on the mechanical properties of the SiCf/SiC composites fabricated by PIP process, Ceram. Int. 36 (2010) 2033-(2037).

DOI: 10.1016/j.ceramint.2010.05.014

Google Scholar

[16] H. J. Yu, X. G. Zhou, W. Zhang, H. X. Peng, C. R. Zhang, Z. L. Huang, Mechanical properties of 3D KD-I SiCf/SiC composites with engineered fibre–matrix interfaces, Compos. Sci. Technol. 71 (2011) 699-704.

DOI: 10.1016/j.compscitech.2011.01.014

Google Scholar

[17] S. Zhao, X. Zhou, J. Yu, P. Mummery, Fabrication and characterization of 2. 5D and 3D SiCf/SiC composites, Fusion Eng. Des. 88 (2013) 2453– 2456.

DOI: 10.1016/j.fusengdes.2013.04.002

Google Scholar

[18] S. Zhao, X. Zhou, J. Yu, P. Mummery, Effect of heat treatment on microstructure and mechanical properties of PIP-SiC/SiC composites, Mater. Sci. Eng. A 559 (2013) 808–811.

DOI: 10.1016/j.msea.2012.09.027

Google Scholar