Microstructure and Interconnections Characteristics of Titanium Foam

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Abstract:

Titanium foams are widely used as biomaterials and potentially as a twin skinned, sandwich, structures for aerospace structures, filter or a catalyst or catalysts carrier for chemical reactions. The porosity is particularly important for tissues ingrowth and vascularity. Open porosity is essential in the case of flow-on machines. The distribution and size of pores is significant to achieve a uniform material effort and ensure to receive an appropriate hydraulic properties.The aim of this study was to determine the effect of titanium particle size and the amount of porogen on the microstructure and the size of pore interconnections in titanium foams made using saccharose as the space holder material.The paper characterizes titanium foam, made from the Grade 1 Ti powders (Alfa Aesar) with a particle sizes of 0.150 mm and 0.044 mm (separately) and spherical particles of saccharose (Pfeifer & Langen) having an average size of 0.7 ÷ 0.9 mm, as a porogen. There was prepared a mixture of powders of the proposed porosity of 50, 60 and 70%. Summarizing 6 mixtures were prepared. After sintering there were received specimens having a diameter of 8 mm and a height of 5 mm. Microstructure analysis was performed using the microtomography Skyscan 1172 (Bruker microCT) and the CTAn software (Bruker microCT).The results indicate the uniform pore distribution and size of the interconnections allowing high permeability.

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25-32

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April 2016

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© 2016 Trans Tech Publications Ltd. All Rights Reserved

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[1] J. Qin, Q. Chen, Ch. Yang, Y. Huang, Research process on property and application of metal porous materials, J. Alloy. Compd. 654 (2016) 39-44.

Google Scholar

[2] R.A.W. Mines, S. Tsopanos, Y. Shen, R. Hasan, S.T. McKown, Drop weight impact behaviour of sandwich panels with metallic micro lattice cores, Int. J. Impact. Eng. 60 (2013) 120-132.

DOI: 10.1016/j.ijimpeng.2013.04.007

Google Scholar

[3] A.S. Hermann, P.C. Zahlen, I. Zuardy, Sandwich structures technology in commercial aviation. In: 7th International Conference on sandwich structures (ICSS-7), Aalborg 2005. pp.13-26.

DOI: 10.1007/1-4020-3848-8_2

Google Scholar

[4] P.S. Liu, H.B. Qing, H.L. Hou, Primary investigation on sound absorption performance of highly porous titanium foams, Mater. Design. 85 (2015) 275–281.

DOI: 10.1016/j.matdes.2015.06.118

Google Scholar

[5] A. Zieliński, S. Sobieszczyk, T. Seramak, W. Serbiński, B. Świeczko-Żurek, A. Ossowska, Biocompatibility and bioactivity of load-bearing metallic implants. Advances in Materials Science, 10 (2010), No. 4 (26), 21-31.

DOI: 10.2478/v10077-010-0013-1

Google Scholar

[6] M. Long, H.J. Rack, Titanium alloys in total joint replacement – materials science perspective, Biomaterials 19 (1998) 1621–1639.

DOI: 10.1016/s0142-9612(97)00146-4

Google Scholar

[7] J. Jakubowicz, G. Adamek, K. Pałka, D. Andrzejewski, Micro-CT analysis and mechanical properties of Ti spherical and polyhedral void composites made with saccharose as a space holder material, Mater. Charact. 100 (2015) 13-20.

DOI: 10.1016/j.matchar.2014.12.006

Google Scholar

[8] E. Vanderleyden, S. Van Bael, Y.C. Chai, J.P. Kruth, J. Schrooten, P. Dubruel, Gelatin functionalised porous titanium alloy implants for orthopaedic applications, Mater. Sci. Eng. C Mater. Biol. Appl. 42 (2014) 396-404.

DOI: 10.1016/j.msec.2014.05.048

Google Scholar

[9] Z. Esen, S. Bor, Processing of titanium foams using magnesium spacer particles, Scripta Mater. 56 (2007) 341–344.

DOI: 10.1016/j.scriptamat.2006.11.010

Google Scholar

[10] A. Mansourighasri, N. Muhamad, A.B. Sulong, Processing titanium foams using tapioca starch as a space holder, J. Mat. Proc. Techn. 212 (2012) 83–89.

DOI: 10.1016/j.jmatprotec.2011.08.008

Google Scholar

[11] A. Bansiddhi, D.C. Dunand, Shape memory NiTi foams produced by solid state replication with NaF, Intermetalics 15 (2007) 1612–1622.

DOI: 10.1016/j.intermet.2007.06.013

Google Scholar

[12] Y. Torres, J.J. Pavón, J.A. Rodríguez, Processing and characterization of porous titanium for implants by using NaCl as space holder, J. Mater. Process. Techn. 212 (2012) 1061–1069.

DOI: 10.1016/j.jmatprotec.2011.12.015

Google Scholar

[13] K. Palka, B. Szaraniec, Microstructural analysis of porosity-graded titanium sinters using microtomography, Eng. Biomater. 112 (2012) 26–30.

Google Scholar

[14] J. Jakubowicz, G. Adamek, M. Dewidar, Titanium foam made with saccharose as a space holder, J. Por. Mater. 20 (2013) 1137–1141.

DOI: 10.1007/s10934-013-9696-0

Google Scholar

[15] R. Singh, P.D. Lee, T.C. Lindley, R.J. Dashwood, E. Ferrie, T. Imwinkelried, Characterization of the structure and permeability of titanium foams for spinal fusion devices, Acta Biomater. 5 (2009) 477–487.

DOI: 10.1016/j.actbio.2008.06.014

Google Scholar

[16] Morphometric parameters measured by Skyscan™ CT Analyser software, http: /www. skyscan. be/next/ctan03. pdf, 2014 (available September, 2015).

Google Scholar