Influence of Hardener Content and Curing Parameters on the Microstructure and Mechanical Properties of Porous C/C Composites

Article Preview

Abstract:

Carbon fibre reinforced carbon composites (C/C) are characterised by their excellent thermal, chemical and mechanical properties. The intrinsic porosity and fibre reinforcement grant them an excellent damage tolerance. The production of complex structures is time consuming and very expensive. An innovative approach to this topic is the integration of simple geometric ceramic composite materials within complex polymer structures. The motivation of this contribution is to investigate the influence of hexamethylenetetramine as hardener (hardener content: 4, 8, 12 and 16 %) and curing parameters (tempered and non-tempered) on the microstructure and mechanical properties of the porous C/C composites. During the course of this contribution, selected carbon fibre reinforced polymer (CFRP) composites with different porosities were produced while adjusting the resin or hardening agent-ratio, as well as the processing parameters. Subsequent to the curing of the CFRP samples, porous C/C composites were produced by means of a pyrolysis process. The final part of the contribution is comprised of the microstructural analysis by light microscopy and the explanation of the flexural strengths, by utilising a “three-point-bending test”.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

246-252

Citation:

Online since:

July 2017

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2017 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Todt, A.; Trautmann, M.; Nestler, D.; Wagner, G.: New approach to design of ceramic/polymer material compounds, Materials Science and Engineering, IOP Publishing Ltd, Vol. 118, 1, p.012015 (2015).

DOI: 10.1088/1757-899x/118/1/012015

Google Scholar

[2] Nestler, D.; Todt, A.; Wielage, B.; Wagner, G.: Fundamental studies and development on an innovative ceramic/polymer material compound, Materials Science Forum, Trans Tech Publications, Switzerland, Vol. 825–826, S. 305–313 (2015).

DOI: 10.4028/www.scientific.net/msf.825-826.305

Google Scholar

[3] Mucha, H.: Untersuchungen zur Porositätsentwicklung von Phenolharzen als polymere-und Kohlenstoffspendermatrices in C-Faserverbundwerkstoffen, Dissertation, TU Chemnitz, (2002).

Google Scholar

[4] DIN EN 1389: 2004-03, Advanced technical ceramics - Ceramic composites - Physical properties - Determination of density and apparent porosity, (2004).

DOI: 10.3403/02984267

Google Scholar

[5] DIN EN 658-3, Advanced technical ceramics - Mechanical properties of ceramic composites at room temperature - Part 3: Determination of flexural strength, (2002).

DOI: 10.3403/02648093u

Google Scholar