Bond Strength of Co-Bonded Thermoplastic Leading Edge Protection (LEP): The Effect of Processing-Driven Interphase Morphology

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Integrated leading edge protection (InLEP) is a novel LEP method that involves co-bonding a tough thermoplastic to the blade shell of the wind turbine made of fiber-reinforced thermoset polymer. In the co-bonding process, as a result of the interdiffusion of the bonded thermoplastic and thermoset polymers, an interphase is formed between them. An important factor affecting the level of interdiffusion is the cure temperature. In this work, we investigate the influence of cure temperature on the interphase morphology and bond strength of ABS-polyester/glass and PC-polyester/glass hybrid composites. The hybrid composites are manufactured via vacuum-assisted resin transfer molding. Interphase morphology is observed and the interphase thickness is measured via optical microscopy. Bond strength is tested via climbing drum peel testing and subsequently, fractography analysis is carried out on the fractured samples. It was found that both the interphase thickness and bond strength decrease with an increase of cure temperature. The decrease in bond strength at high temperatures was accompanied by an increase in the extent of interfacial failure, while interphase failure at low temperatures promoted higher bond strength.

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1786-1794

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July 2022

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[1] L. Mishnaevsky, Current Challenges of Wind Energy Development: Materials Science Aspects, Phys. Mesomech. 24 (2021) 533–540.

DOI: 10.1134/s1029959921050040

Google Scholar

[2] R. Herring, K. Dyer, F. Martin, C. Ward, The increasing importance of leading edge erosion and a review of existing protection solutions, Renew. Sustain. Energy Rev. 115 (2019) 109382.

DOI: 10.1016/j.rser.2019.109382

Google Scholar

[3] M.D. Haag, U.S. Patent US20180209400A1. (2018).

Google Scholar

[4] S. Deng, L. Djukic, R. Paton, L. Ye, Thermoplastic – epoxy interactions and their potential applications in joining composite structures – A review, Compos. Part A Appl. Sci. Manuf. 68 (2015) 121–132.

DOI: 10.1016/j.compositesa.2014.09.027

Google Scholar

[5] L.J. Vandi, M. Hou, M. Veidt, R. Truss, M. Heitzmann, R. Paton, Interface diffusion and morphology of aerospace grade epoxy co-cured with thermoplastic polymers, ICAS 2012 28th Congr. Int. Counc. Aeronaut. Sci. (2012).

Google Scholar

[6] J.S.M. Zanjani, I. Baran, R. Akkerman, Characterization of interdiffusion mechanisms during co-bonding of unsaturated polyester resin to thermoplastics with different thermodynamic affinities, Polymer 209 (2020) 122991.

DOI: 10.1016/j.polymer.2020.122991

Google Scholar

[7] J.S.M. Zanjani and I. Baran, Co-Bonded Hybrid Thermoplastic-Thermoset Composite Interphase: Process-Microstructure-Property Correlation, Materials 14 (2021) 291.

DOI: 10.3390/ma14020291

Google Scholar

[8] L. Zweifel and C. Brauner, Investigation of the interphase mechanisms and welding behaviour of fast-curing epoxy based composites with co-cured thermoplastic boundary layers, Compos. Part A Appl. Sci. Manuf. 139 (2020) 106120.

DOI: 10.1016/j.compositesa.2020.106120

Google Scholar

[9] O. Erartsın, J.S.M. Zanjani, L. Chu, I. Baran, Unravelling the interphase morphology - bond strength relationship in novel co-bonded thermoplastic - thermoset hybrid composites for leading edge protection of wind turbine blades, Manuscript submitted for publication (2022).

DOI: 10.1016/j.polymertesting.2022.107856

Google Scholar

[10] ASTM D1781 - 98 Standard Test Method for Climbing Drum Peel for Adhesives.

Google Scholar

[11] J. Cañas, L. Távara, A. Blázquez, A. Estefani, G. Santacruz, A new in situ peeling test for the characterisation of composite bonded joints, Compos. Part A Appl. Sci. Manuf. 113 (2018) 298–310.

DOI: 10.1016/j.compositesa.2018.07.014

Google Scholar

[12] F. Daghia and C. Cluzel, The Climbing Drum Peel Test: An alternative to the Double Cantilever Beam for the determination of fracture toughness of monolithic laminates, Compos. Part A Appl. Sci. Manuf. 78 (2015) 70-83.

DOI: 10.1016/j.compositesa.2015.07.010

Google Scholar

[13] I.F. Villegas and R. van Moorleghem, Ultrasonic welding of carbon/epoxy and carbon/PEEK composites through a PEI thermoplastic coupling layer, Compos. Part A Appl. Sci. Manuf. 109 (2018) 75–83.

DOI: 10.1016/j.compositesa.2018.02.022

Google Scholar