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Preparation and Characterization of Nickel Complex [Ni(1-MeIm)6(BF4)2] in Ionic Liquid

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Abstract:

Nickel complex [Ni(1-MeIm)6(BF4)2, 1-MeIm = 1-methylimidazole] has been prepared in 1-butyl-3-methylimidazolium tetrafluoroborate ([bmim]BF4) ionic liquid by a simple solution phase method. The complex was characterized by elemental analysis, X-ray diffraction (XRD), scanning electron microscopy (SEM), infrared absorption spectroscopy (IR) and thermal analysis. SEM image indicates that the complex is irregular platelets with an uneven thickness in nanometer scale and variable transverse and longitudinal size, from 0.6 to 4 μm.

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Periodical:

Materials Science Forum (Volumes 663-665)

Pages:

1167-1170

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.663-665.1167

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Cite this paper

Online since:

November 2010

Authors:

Jun Sai Sun, Cun Ying Xu

Keywords:

1-Methylimidazole, Ionic Liquid (IL), Nickel Complex, Synthesis

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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