Containerless Solidification of Eutectic PbSn Alloy Droplets in a Drop Tube

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Abstract:

Containerless solidification of 300 to 850 µm diameter droplets of PbSn eutectic alloy was achieved by using a 3m length drop tube, which is one of the most suitable and low cost option to provide a microgravity environment on the ground. Phase morphology and composition were investigated, respectively, by scanning electron microscopy (SEM) and energy dispersive spectrometry (EDS). It was found that the microstructure of the droplets depends on their sizes, where in larger diameters (>500µm) consists of both regular lamellar and irregular structures, and on other hand, for the smaller ones (<500µm) the structure is only irregular with higher lead concentration.

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Materials Science Forum (Volumes 727-728)

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1633-1637

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August 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] H.U. Walter (Ed. ). Fluid sciences and materials science in space: An European Perspective. -. Berlin, Germany: Springer, (1987).

Google Scholar

[2] C.Y. An, I.N. Bandeira, C. Boschetti, R.C. Toledo and M.B. de Mattos. Drop tube for containerless solidification under microgravity environment. Sixth International Latin American Conference on Powder Technology (PTECH). Búzios, 07-10 de Novembro 2007. Procceding.. Búzios 2007. (RJ).

Google Scholar

[3] R.C. Toledo, M.B. Mattos, C.Y. An and I.N. Bandeira: Mater. Sci. Forum Vols. 660-661 (2010), p.587.

Google Scholar

[4] E. Cadırl, D.M. Herlach and T. Volkmann: Journal of Non-Crystalline Solids Vol. 356 (2010).

Google Scholar

[5] R.C. Toledo, F.E. Freitas, C.Y. An and I.N. Bandeira. Cálculo de densidade de ligas eutéticas binárias. 2º Workshop em Engenharia e Tecnologia Espaciais., São José dos Campos, 2011. Proceeding.. São José dos Campos 2011. (SP).

DOI: 10.14393/19834071.2014.26671

Google Scholar

[6] C.Y. An, I.N. Bandeira, D.M. Rowe and G. Min.: Jounal of Materials Science Letters Vol. 13 (1994), p.1051.

Google Scholar

[7] C.Y. An, C.R. M da Silva and D.M. Rowe: Materials Letters Vol. 28 (1996), p.83.

Google Scholar

[8] Information on http: /www. americanelements. com/biinsn. html.

Google Scholar

[9] W. Kurz, D.J. Fisher. Fundamentals of Solidification, 4th Edition, Trans Tech Publications Ltd., Uetikon-Zuerich, Switzerland, (1998).

Google Scholar

[10] D. Herlach; P. Galenko; D. Holland-Moritz. Metastable Solids from Undercooled Melts, Pergamon Materials Series-Elsevier, Oxford, UK, (2007).

DOI: 10.1016/s1470-1804(07)80023-x

Google Scholar