Paper Title:
Natural Rubber Based Compatibilizer Prepared in Twin Screw Extruder: Optimization Percentage of Grafted Maleic Anhydride Using Experimental Design
  Abstract

Maleic anhydride grafted natural rubber compatibilizer was prepared in molten state using twin screw extruder. Amount of maleic anhydride and initiator, as well as screw rotation were varied according to Box-Behnken experimental design. Titration of acid group from the anhydride function and FTIR spectra analysis were carried out as quantitative and qualitative analysis of grafted MA, respectively. The results showed that the percentages of grafted MA for all samples were ranged from 1.31 to 5.36%. The optimum conditions are predicted at 14.4 phr of MA level, 0.41 phr of BPO level, and 71 rpm screw rotation giving 5.39 ± 0.16% of grafted MA. FTIR spectra showed that the MA and carbonyl functional group were found in the compatibilizer suggested the presence of grafted MA and ring opening reaction.

  Info
Periodical
Chapter
Chapter 1: Polymers and Composites
Edited by
Tjokorda Gde Tirta Nindhia, Hendra Suherman, Brian Yuliarto
Pages
13-17
DOI
10.4028/www.scientific.net/MSF.864.13
Citation
O. Ujianto, Marzuki, F. A. Radini, "Natural Rubber Based Compatibilizer Prepared in Twin Screw Extruder: Optimization Percentage of Grafted Maleic Anhydride Using Experimental Design", Materials Science Forum, Vol. 864, pp. 13-17, 2016
Online since
August 2016
Export
Price
$35.00
Share
* Corresponding Author

In order to see related information, you need to Login.

In order to see related information, you need to Login.

Authors: L.H. Chou, L.K Lin, M.T. Lee
Abstract:Polypropylene (PP) fiber reinforced concrete is an important composite. In order to improve the mechanical properties of PP fiber reinforced...
1693
Authors: Xia Xu, Tie Ling Xing, Guo Qiang Chen
Abstract:In this work, silk was grafted using dimethylaminoethyl methacrylate(DMAEMA) via activators regenerated by electron transfer for atom...
608
Authors: Shan Hu, Hu Liang Gao, Jun Zhang
Chapter 1: Smart Materials and Nanotechnology
Abstract:The grafted starch was prepared from corn starch and maleic anhydride. Fourier transform infrared spectroscopy (FTIR) was used to...
70
Authors: Li Na Wang, Xian Lin Xu, Yuan Lin Ren, Xiao Yang Sui
Chapter 2: Technology in Textile Industry
Abstract:The graft copolymerization of acrylamide onto polyester-cotton blended (PCB) fabric by using potassium permanganate (KMnO4) redox system was...
205