A Direct Route to Active Silica Nanoparticles

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Abstract:

Monodisperse silica particles containing available active C=C bonds were directly prepared by a simple two-step sol-gel method. In the first step the hydrolysis of vinyltrimethoxysilane (VTMS) was performed under acidic conditions in an aqueous solution. In the second step the condensation of the siloxane precursors progressed under basic conditions, resulting in production of silica nanoparticles containing available active C=C bonds. The products were characterized using SEM and FTIR.

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Solid State Phenomena (Volumes 121-123)

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65-68

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March 2007

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© 2007 Trans Tech Publications Ltd. All Rights Reserved

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[1] T. Ysnsgishita, Y. Tomabechi, K. Nishio and H. Masuda: Langmuir Vol. 20(2004), p.554.

Google Scholar

[2] C.A.R. Costa, C.A.P. Leite, and F. Galembeck: J. Phys. Chem. B Vol. 107(2003), p.4747.

Google Scholar

[3] M. Chen, L.M. Wu, S.X. Zhou and B. You: Macromolecules Vol. 37(2004), p.9613.

Google Scholar

[4] J.H. Hoe and M.K. Sang: J. Sol-Gel Sci. Techn. Vol. 31(2004), p.117.

Google Scholar

[5] W. Stöber, A. Fink and E. Bohn: J. Colloid Interf. Sci. Vol. 26(1968), p.62.

Google Scholar

[6] S. Nozaki, K. Uchida, H. Morisaki, T. Kawasaki and M. Ibukiyama: JKXXAF JP, 2004331480 A2 20041125(2004).

Google Scholar

[7] A. van Blaaderen and A. Vrij: J. Colloid Interf. Sci. Vol. 156(1993), p.1.

Google Scholar

[8] G. Hernandez-Padron, F. Rojas and V.M. Castano: Nanotechnology Vol. 15(2004), 98.

Google Scholar

[9] A. Bertoluzza, C. Fagnano and M.A. Morelli: J. Non-Cryst. Solids Vol. 48(1982), p.117.

Google Scholar

[10] M. Zaharescu, A. Jitianu, A. Braileanu, J. Madarasz and G. Pokol: J. Thermanal Anal. Calorim. Vol. 64(2001), p.689.

DOI: 10.1023/a:1011536209930

Google Scholar

[11] Q. Deng, K.A. Mauritz and R.B. Moore: Hybrid Organic-Inorganic Composites, ACS Symposium Series (1995), p.585.

Google Scholar

[12] C.A. Capozzi, L.D. Pye and R.A. Condrate: Mater. Lett. Vol. 15(1992), p.130.

Google Scholar