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Online since: November 2011
Authors: Chang Jian Xiong, Ji Ne Wang, Yue Lin Zhu
Synthesis and Characterization of Iso E Super®
Yuelin ZHU1, a, Jine WANG2, b, Changjian XIONG3, c
1 School of Material Science and Engineering, Beihang University, Beijing, China
2 School of Material Science and Engineering, Beihang University, Beijing, China
3 School of Material Science and Engineering, Beihang University, Beijing, China
aylzhu@buaa.edu.cn, bsdwangjine@yahoo.cn, cxchj@buaa.edu.cn
Keywords: Aldol condensation; diene synthesis; cyclization; Iso E Super®; organic synthesis ; ambergris
Abstract.
The method used has the advantages of readily availability of starting materials, mild reaction conditions, convenient manipulation and moderately high yields, so it has a promising prospect in industrial production Introduction 1-(1,2,3,4,5,6,7,8-Octahydro-2,3,8,8-tetramethyl-2-naphthalenyl)ethanone, commonly referred to as Iso E Super®[1], is a an important synthetic perfume for its stability and unique properties[2].
Fig1.Synthetic route of Iso E Super® 2 Experimental 2.1 Materials and instruments Main materials: aldehyde, butanone (C.P.), myrcene; catalytic agent:KOH, AlCl3, H3PO4, oxalic acid; Solvent: Toluene (C.P.).
Column chromatography was performed using silica gel 60 (0.063–0.200 nm). 2.2 Materials preparation Myrcene was supplied by a corporation in the Guangxi Zhuang Autonomous Region of China.
Journal of Molecular Catalysis A: Chemical 1999, 148, 87-95
The method used has the advantages of readily availability of starting materials, mild reaction conditions, convenient manipulation and moderately high yields, so it has a promising prospect in industrial production Introduction 1-(1,2,3,4,5,6,7,8-Octahydro-2,3,8,8-tetramethyl-2-naphthalenyl)ethanone, commonly referred to as Iso E Super®[1], is a an important synthetic perfume for its stability and unique properties[2].
Fig1.Synthetic route of Iso E Super® 2 Experimental 2.1 Materials and instruments Main materials: aldehyde, butanone (C.P.), myrcene; catalytic agent:KOH, AlCl3, H3PO4, oxalic acid; Solvent: Toluene (C.P.).
Column chromatography was performed using silica gel 60 (0.063–0.200 nm). 2.2 Materials preparation Myrcene was supplied by a corporation in the Guangxi Zhuang Autonomous Region of China.
Journal of Molecular Catalysis A: Chemical 1999, 148, 87-95
Online since: November 2015
Authors: Carmen Debeleac, Cristian Simionescu, Silviu Nastac
[5] Leng, C.Q., Huang, Y.L., Analyses the Mechanical Equipment Management and Maintenance, Applied Mechanics and Materials, Vols. 599-601, pp. 2066-2069, Aug. (2014)
[6] Li, Y.H., Nie, L.X., Ding, S., Large-Scale Construction Equipment Joint Simulation Based on Multi-Body Dynamics Theory, Advanced Materials Research, Vols. 268-270, pp. 101-105, Jul. (2011) [7] Margolis, D., Shim, T., Instability Due to Interacting Hydraulic and Mechanical Dynamics in Backhoes, Journal of Dynamic Systems, Measurement and Control, ASME, Vol. 125, pp. 497-504, (2003)
[8] Olaru, A., Olaru, S., Mihai, N., Proper Smart Method of the Inverse Kinematic Problem, Applied Mechanics and Materials, Vol. 772, pp. 455-460, Jul. (2015)
[9] Olaru, A., Olaru, S., Mihai, N., Proper Assisted Research Method Solving of the Robots Inverse Kinematics Problem, Applied Mechanics and Materials, Vol. 555, pp. 135-146, Jun. (2014) [10] Rao, S.S., Bhatti, P.K., Probabilistic approach to manipulator kinematics and dynamics, Reliability Engineering and System Safety, Elsevier Science, Vol. 72, pp. 47-58, (2001)
[12] Topliceanu, L., Ghenadi, A.S., Bibire, L., Elements of Design and Dimensioning of Hydraulic System with Secondary Control, Applied Mechanics and Materials, Vol. 436, pp. 137-144, Oct. (2013) [13] Zhang, L., Analysis of Construction Machinery Hydraulic Control System, Applied Mechanics and Materials, Vols. 401-403, pp. 1590-1595, Sep. (2013) [14] Zhong, X.Q., Liang, L.D., Mechanical-Hydraulic Coupling Simulation for Hydraulic Excavator Working Mechanism, Advanced Materials Research, Vols. 538-541, pp. 494-497, Jun. (2012).
[6] Li, Y.H., Nie, L.X., Ding, S., Large-Scale Construction Equipment Joint Simulation Based on Multi-Body Dynamics Theory, Advanced Materials Research, Vols. 268-270, pp. 101-105, Jul. (2011) [7] Margolis, D., Shim, T., Instability Due to Interacting Hydraulic and Mechanical Dynamics in Backhoes, Journal of Dynamic Systems, Measurement and Control, ASME, Vol. 125, pp. 497-504, (2003)
[8] Olaru, A., Olaru, S., Mihai, N., Proper Smart Method of the Inverse Kinematic Problem, Applied Mechanics and Materials, Vol. 772, pp. 455-460, Jul. (2015)
[9] Olaru, A., Olaru, S., Mihai, N., Proper Assisted Research Method Solving of the Robots Inverse Kinematics Problem, Applied Mechanics and Materials, Vol. 555, pp. 135-146, Jun. (2014) [10] Rao, S.S., Bhatti, P.K., Probabilistic approach to manipulator kinematics and dynamics, Reliability Engineering and System Safety, Elsevier Science, Vol. 72, pp. 47-58, (2001)
[12] Topliceanu, L., Ghenadi, A.S., Bibire, L., Elements of Design and Dimensioning of Hydraulic System with Secondary Control, Applied Mechanics and Materials, Vol. 436, pp. 137-144, Oct. (2013) [13] Zhang, L., Analysis of Construction Machinery Hydraulic Control System, Applied Mechanics and Materials, Vols. 401-403, pp. 1590-1595, Sep. (2013) [14] Zhong, X.Q., Liang, L.D., Mechanical-Hydraulic Coupling Simulation for Hydraulic Excavator Working Mechanism, Advanced Materials Research, Vols. 538-541, pp. 494-497, Jun. (2012).
Online since: August 2009
Authors: Xi Peng Xu, Cong Fu Fang
Introduction
Sawing with segmented diamond sawblades is the most widely used process for natural stone and
other construction materials.
Many previous studies on the grinding of brittle materials with diamond mentioned the dependence of tool wear on the temperatures generated in the wheel-workpiece contact zone [1].
For grinding and sawing of granite materials, however, what is of most concern is the wear of the diamond tools rather than the thermal damage to the workpiece.
Luo: Journal of Materials Science Vol. 1245(51) (1993), p. 28 [3] W.
Xu: Key Engineering Materials Vol. 375-376 (2008), p. 549 [8] W.B.
Many previous studies on the grinding of brittle materials with diamond mentioned the dependence of tool wear on the temperatures generated in the wheel-workpiece contact zone [1].
For grinding and sawing of granite materials, however, what is of most concern is the wear of the diamond tools rather than the thermal damage to the workpiece.
Luo: Journal of Materials Science Vol. 1245(51) (1993), p. 28 [3] W.
Xu: Key Engineering Materials Vol. 375-376 (2008), p. 549 [8] W.B.
Online since: July 2014
Authors: Shabnam Hosseini, Mohammad Bagher Limooei
Methods and Materials
In the present study, cylindrical specimens of Hadfield steel were used.
Srivastava, K.Das, “Microstructural Characterization of Hadfield Austenitic Manganese Steel”, Materials Sciences, 2008, Vol. 43, pp.5654-5658
Song, “Eutectic Decomposition in Ca-Si Modified Austenitic Medium Mn Steel after Solidification”, Materials Sciences, 2005, Vol. 40, pp. 2081-2084
[12] P.W.Mason and P.S.Prevey, “Iterative Taguchi Analysis: optimizing the austenite content and hardness in 52100 steel”, Journal of Materials Engineering and performance, Vol. 10(1), February 2001,14-21
Tagore, “Experimental investigation on flow-forming of AA6061 alloy-A Taguchi approach”, journal of materials processing technology , 2008(200): 283–287 [14] Adem Cicek, Turgay Kivak, Gurcan Samtas, “Application of Taguchi Method for Surface Roughness and Roundness Error in Drilling of AISI 316 Stainless Steel”,Journal of Mechanical Engineering, 58(2012)3, 165-174.
Srivastava, K.Das, “Microstructural Characterization of Hadfield Austenitic Manganese Steel”, Materials Sciences, 2008, Vol. 43, pp.5654-5658
Song, “Eutectic Decomposition in Ca-Si Modified Austenitic Medium Mn Steel after Solidification”, Materials Sciences, 2005, Vol. 40, pp. 2081-2084
[12] P.W.Mason and P.S.Prevey, “Iterative Taguchi Analysis: optimizing the austenite content and hardness in 52100 steel”, Journal of Materials Engineering and performance, Vol. 10(1), February 2001,14-21
Tagore, “Experimental investigation on flow-forming of AA6061 alloy-A Taguchi approach”, journal of materials processing technology , 2008(200): 283–287 [14] Adem Cicek, Turgay Kivak, Gurcan Samtas, “Application of Taguchi Method for Surface Roughness and Roundness Error in Drilling of AISI 316 Stainless Steel”,Journal of Mechanical Engineering, 58(2012)3, 165-174.
Online since: November 2012
Authors: Zhan Guo Xu, Dong Ju Feng
It is best suited for machining hard, brittle materials [1-3].
Since the tool is usually made of metal materials, the mechanism of tool wear is different from the removal mechanism of the workpiece.
References [1] H.Hocheng, K.L.Kuo: Journal of Materials Processing Technology, Vol.123(2002), p.80-84
[4] LIU Yao,JI Xiao-me: Journal of electric power, Vol.24(2009), p. 402-404
[7] T.C.Lee, C.W.Chan: Journal of materials processing technology , Vol.71(1997), p. 195-201 [8] Adithan M.: Tribology International, Vol.14(1981), p. 351-356
Since the tool is usually made of metal materials, the mechanism of tool wear is different from the removal mechanism of the workpiece.
References [1] H.Hocheng, K.L.Kuo: Journal of Materials Processing Technology, Vol.123(2002), p.80-84
[4] LIU Yao,JI Xiao-me: Journal of electric power, Vol.24(2009), p. 402-404
[7] T.C.Lee, C.W.Chan: Journal of materials processing technology , Vol.71(1997), p. 195-201 [8] Adithan M.: Tribology International, Vol.14(1981), p. 351-356
Online since: May 2011
Authors: Ji Shun Song, Yun Tao Li, Juan Ye, Jin Kui Wang, Jian Zhang
Study on microstructure and formability of laser tailor-welded joints of aluminum alloy thin sheet
Yuntao Li1,2,a , Juan Ye1, b, Jinkui Wang3, c, Jishun Song1,2,d and Jian Zhang1,2,e
1School of Materials Science & Engineering, Tianjin University of Technology, Tianjin, 300384,China
2Tianjin Key Laboratory for Photoelectric Display Materials and Devices, Tianjin 300384,China
3TIANJIN MOTOR DIES CO., LTD.
Experimental Material and Method Experimental Materials.
Materials Science and Engineering A, 2000, 280 (3) : 37-49
Journal of Materials Processing Technology, 2000, 99 (1): 145- 153
Materials and Design, 2004, 25: 573 - 577.
Experimental Material and Method Experimental Materials.
Materials Science and Engineering A, 2000, 280 (3) : 37-49
Journal of Materials Processing Technology, 2000, 99 (1): 145- 153
Materials and Design, 2004, 25: 573 - 577.
Online since: June 2008
Authors: Gabriela Botelho, Senentxu Lanceros-Méndez, Michael Belsley, Jivago Serrado-Nunes, A.M. Gonçalves, Vitor Sencadas
Introduction
One major problem associated with the applications of polymers is their instability to weathering
(light, temperature….) which results in a degradation of the properties of the exposed materials.
Pouzada: Materials Science Forum, Vol. 514 - 516 (2006), p. 872 [5] V.
Lanceros-Mendez: Journal of Non-Cristalline Solids, Vol. 21-22 (2006), p. 2226 [6] P.
Rocha: Journal of Non Crystalline Solids Vol. 354 (2008), p. 72
Science Vol. 70 (1998), p. 1471.
Pouzada: Materials Science Forum, Vol. 514 - 516 (2006), p. 872 [5] V.
Lanceros-Mendez: Journal of Non-Cristalline Solids, Vol. 21-22 (2006), p. 2226 [6] P.
Rocha: Journal of Non Crystalline Solids Vol. 354 (2008), p. 72
Science Vol. 70 (1998), p. 1471.
Online since: November 2011
Authors: Bing Xie, Jin Jun Guo, Xiang Xia
Germanovich[3,4] and Wong [5,6] conducted uniaxial compression test by using specimens with several 3-D shape flaws which made of organic glass and other brittle materials and analyzed the impact of flaws on the mechanical properties.
Natural rock is a typical non-homogeneous material and it often contains different kind of flaws such as joints.
Tang:Mechanics of Materials, Vol.38(2006),p.142 [6] R.H.C.
Cundall: International Journal of Rock Mechanics & Mining Sciences Vol.41(2004), p.1329 [9] N.
Sego: International Journal of Rock Mechanics and Mining Sciences, Vol. 44(2007), p.997
Natural rock is a typical non-homogeneous material and it often contains different kind of flaws such as joints.
Tang:Mechanics of Materials, Vol.38(2006),p.142 [6] R.H.C.
Cundall: International Journal of Rock Mechanics & Mining Sciences Vol.41(2004), p.1329 [9] N.
Sego: International Journal of Rock Mechanics and Mining Sciences, Vol. 44(2007), p.997
Online since: September 2015
Authors: Ya Yan Gao, Li Gang Zhai, Li Xin Wang, Li Qiang Peng
At present, more researches have been done on the change of materials than the surface structure to improve the brake disc performance.
Set the materials of the brake disc and friction plates, as brake disc is HT200, friction plates are resin with reinforced composite materials.
Zhu, Research and discussion on mechanism of brake heat fading caused by friction materials, J.
Journal of Xihua University · Natural Science. 31 (2012) 31-34
Journal of Jilin University (Earth Science Edition). 42 (2012) 220-225
Set the materials of the brake disc and friction plates, as brake disc is HT200, friction plates are resin with reinforced composite materials.
Zhu, Research and discussion on mechanism of brake heat fading caused by friction materials, J.
Journal of Xihua University · Natural Science. 31 (2012) 31-34
Journal of Jilin University (Earth Science Edition). 42 (2012) 220-225
Online since: January 2012
Authors: Zhi Gang Song, Hong Guang Min, Xue Song Zhang
In general, compared with the carbonation and chloride attacking, the mechanism of sulfuric acid corroding concrete materials is more complex.
Shanghai Environmental Sciences, 1991(1):37-39.
ASCE: Journal of materials in civil engineering, Vol.11, 1999(4):340-344.
Journal of materials science, Vol.32, 1997: 4109-4116
ASCE: Journal of materials in civil engineering, 2007(2):155-63
Shanghai Environmental Sciences, 1991(1):37-39.
ASCE: Journal of materials in civil engineering, Vol.11, 1999(4):340-344.
Journal of materials science, Vol.32, 1997: 4109-4116
ASCE: Journal of materials in civil engineering, 2007(2):155-63