Authors: Yu Li Sun, Dun Wen Zuo, W.Z. Lu, Y.W. Zhu, J. Li
Abstract: The ice fixed abrasives (IFA) polishing is a potential polishing process in the semiconductor industry to realize superior surface finish and planarity for semiconductor wafers. The key question in IFA polishing is how to keep suitable ambient temperature and melting rate in production process in order to avoid premature failure of the IFA pad. In this paper, effects of ambient temperature (T), pressure in cylinder (Pc), rotary speed of IFA pad (v) and eccentricity of pressure head (e) on temperature distribution and melting rate of the IFA pad are researched. The results show that T should be kept at about 10 °C in order to control the melting rate of the IFA pad effectively and keep longer polishing time. And suitable Pc, e can be kept at 0.075 MPa or 0.1 MPa and 20 mm or 30 mm, respectively. In order to increase IFA polishing efficiency, the rotary speed of IFA pad can be increased appropriately. All the results provide the basis for choosing suitable processing parameters in IFA polishing.
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Authors: Yu Li Sun, Dun Wen Zuo, Wen Zhuang Lu, Yu Fei Zhao, Jing Kang, Min Wang
Abstract: The key question in the ice fixed abrasives (IFA) polishing is how to keep suitable ambient temperature in production process in order to avoid premature failure of the IFA. Based on above, the three dimensions finite element analysis (FEA) model of IFA polishing temperature field is built up at first. Then, the model reliability is demonstrated by experiments. Effects of ambient temperature and polishing time on temperature distribution and melting rate of the IFA pad are researched. The results show that the ambient temperature should be kept at about 10 °C in order to control the melting rate of the IFA pad effectively and keep longer polishing time. All the results provide the basis for choosing suitable ambient temperature in polishing.
1
Authors: Yu Li Sun, Dun Wen Zuo, Jun Li, Wen Zhuang Lu, Z.Z. Yu
Abstract: Ice fixed abrasives (IFA) polishing is a novel ultra-precision machining method. The motion tracks of abrasives during IFA polishing have an important effect on the quality of the machined silicon wafer. Firstly, the motion tracks of IFA polishing are theoretically analyzed in this paper. It is founded that the paths of any point in the IFA polishing pad relative to the wokpiece are a group of cycloids. Then, the motion tracks of single abrasive and multiple abrasives in the IFA polishing pad are simulated respectively. The results show that increasing the eccentricity is beneficial to the enlargement of the size range of polishing process. With the increasing of the speed ratio between the IFA polishing pad and the workpiece, the abrasive at higher speed can leave longer tracks on the workpiece than that at lower speed at the same time. The more the abrasives, the more uniform the mark density under the influence of more abrasives.
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Authors: Yu Li Sun, Dun Wen Zuo, Yong Wei Zhu, Ming Wang, H.Y. Wang, Li Gang Zhao
Abstract: The friction behavior of single silicon wafer sliding against different ice counterparts
(α-Al2O3, CeO2 and SiO2) at 10±0.5 °C within a velocity of 60 rpm~300 rpm were studied using a
home-made friction and wear testing machine. The morphologies and surfaces roughness of the worn
silicon wafers were observed and examined on a non-contact surface topography instrument (ADE). It
was found that the friction coefficient of the single silicon wafer decreased with the increase of sliding
velocity. Single crystal silicon wafer coupled with α-Al2O3 ice counterpart recorded the highest
friction coefficient and the biggest surface roughness, while it had the lowest friction coefficient and
the smallest surface roughness as with CeO2 ice counterpart. One reason was that a series of
tribochemical reactions occurred at the local contact point between the ice counterpart and the silicon
wafer during sliding. Under alkaline condition, there would be a soft corrosion layer formed on the
surface of the silicon wafer. Another reason was that the hardness of the abrasive particles was
different and this caused different cutting depth of them.
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Authors: Yu Li Sun, Dun Wen Zuo, Duo Sheng Li, Rong Fa Chen, Min Wang
Abstract: Hardness, elastic modulus and scratch resistance of single silicon wafer are measured by
nanoindentation and nanoscratching using a nanoindenter. Fracture toughness is measured by
indentation using a Vickers indenter. The results show that the hardness and elastic modulus at a peak
indentation depth of 100 nm are 12.6 and 166.5 GPa respectively. These values reflect the properties
of the silicon wafer, the bulk material. The fracture toughness value of the silicon wafer is 0.74
Mpa·m1/2. The material removal mechanisms are seen to be directly related to the normal force on the
tip. The critical load and scratch depth estimated from the scratch depth profile after the scratching
and the friction profile are 138.64 mN and 54.63 nm respectively. If the load and scratch depth are
under the critical values, the silicon wafer will undergo plastic flow rather than fracture. The critical
scratch depth is different from that calculated from the formula of critical-depth-of-cut described by
Bifnao et al and some reasons are given.
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Authors: Yu Li Sun, Dun Wen Zuo, Yong Wei Zhu, Duo Sheng Li, Mei Qi, Min Wang
Abstract: Formation, propagation and length of crack and hardness of single silicon wafer were
investigated at different temperatures by means of Vickers indentation, using lower temperature
testing unit with semiconductor refrigerating chip and higher temperature testing unit with closed
electric furnace. The results show that the hardness of single silicon wafer decreases with the increase
of temperature, while the length of crack increases with the increase of temperature. Ductile-brittle
transition of the single silicon wafer can occur at different temperatures with the increase of load.
When the load is smaller and temperature is lower, no cracks can be found.
1
Authors: Yu Li Sun, Dun Wen Zuo, Yong Wei Zhu, Rong Fa Chen, D.S. Li, M. Wang
Abstract: Cryogenic polishing single silicon wafer with nano-sized CeO2 abrasives can be known as
cryogenic fixed abrasives CMP (CFA-CMP). The abrasive slurry was made of nano-sized CeO2
particles dispersed in de-ionized water with a surfactant and the polishing slurry froze to form
cryogenic polishing pad. Then the polishing tests of the blanket silicon wafers in the presence of the
cryogenic polishing pad containing the nano-particulates were carried out. The morphologies and
surfaces roughness of the polished silicon wafers were observed and examined on an atomic force
microscope (AFM). The results show that a super smooth surface with roughness of 0. 293 nm is
obtained within 5000 nm× 5000 nm and the removal of material is dominated by plastic flowage.
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