Preparation and Characterization of 1-methyl-3-butyl Nitrate

Abstract:

1-methyl-3-butyl Imidazole chloride is prepared by 1–methyl imidazole and chlorinated n-butane. The synthesis reaction of 1-methyl-3-butyl imidazole tetrafluoroborate is in the acetone. The solubility of NaNO₃ and BMIC in acetone is not large, but due to the insolubility in acetone of reaction product NaCl and continuous precipitation from the liquid phase in the reaction process, so as to promote the reaction continuously towards forward direction. The colorless transparent and odorless BMINO₃ are gotten. We use infrared spectrometer for the structure characterization, it is proved that we have gotten BMINO₃ room temperature ionic liquids. BMIC and BMINO₃ ionic liquids have better solubility in H₂O, ethanol, ethyl acetate, acetone, acetonitrile, and methanol, and is insoluble in the ether and cyclohexane.

• Periodical: Applied Mechanics and Materials (Volumes 303-306)
• Pages: 2675-2678
• DOI: https://doi.org/10.4028/www.scientific.net/AMM.303-306.2675
• Online since: February 2013
• Authors: Peng Tian, Yan Hong Kang, Zhi Gang Zhao, Tian Ling Qin, Bo Meng, Wen Le Du
• Keywords: BMIC-NO₃ Ionic Liquid, Characterization, IR-Spectrum, Synthesis

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