Synthesis of Lithium-Ion Battery Cathode Material LiFe0.95Mn0.05PO4/C Using FeCl3 Etching Waste as Iron Source

Guang Hui Guo; Shan Chen; Fang Fang Liu; Li Yu Zhang

doi:10.4028/www.scientific.net/AMM.457-458.191

Paper Titles

The Process Experimental Study on High Efficiency Deep Grinding for 9SiCr Alloy Steel with a CBN Wheel
p.172

Study on the Texture of Materials in Stop Motion
p.177

The DFT Studies on a Novel Hydrogen Storage Material Mg₁₂Ni_6-xCr_x(x=0,1)
p.181

Calculations and Modeling of Material Constants in Hyperbolic-Sine Creep Model for 316 Stainless Steels
p.185

Synthesis of Lithium-Ion Battery Cathode Material LiFe_0.95Mn_0.05PO₄/C Using FeCl₃ Etching Waste as Iron Source
p.191

Novel Anticaking Materials of Bentonite, Biological Carbon and Abandoned Animal/Plant Oil in Compound Fertilizer
p.197

Hydrothermal Synthesis and Investigation of Photocatalytic Properties of Fe-N Co-Doped NaTaO₃
p.202

Preparation and Properties of Cf-Ti₃SiC₂-Cu-Graphite Composites
p.206

Investigation on the Effect of Complexing Agents and Concentrations on Electrodeposition of ZnS Film
p.211

HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vols. 457-458Synthesis of Lithium-Ion Battery Cathode Material...

Synthesis of Lithium-Ion Battery Cathode Material LiFe_0.95Mn_0.05PO₄/C Using FeCl₃ Etching Waste as Iron Source

Abstract:

In this paper, LiFe_0.95Mn_0.05PO₄/C was prepared by using simulated FeCl₃ etching waste as iron source for lithium-ion battery cathode materials. The structural and morphological properties of the samples were characterized by X-ray powder diffraction (XRD) and Scanning electron microscopy (SEM). The electrochemical performances of the sample were also investigated with charge and discharge test. The achieved results indicate that product obtained was confirmed to be LiFe_0.95Mn_0.05PO₄and has the advantage of high purity, small size and good electrochemical performance.

You might also be interested in these eBooks

Frontiers of Mechanical Engineering and Materials Engineering II

View Preview

Info:

Periodical:

Applied Mechanics and Materials (Volumes 457-458)

Pages:

191-196

DOI:

https://doi.org/10.4028/www.scientific.net/AMM.457-458.191

Citation:

Cite this paper

Online since:

October 2013

Authors:

Guang Hui Guo, Shan Chen, Fang Fang Liu, Li Yu Zhang

Keywords:

Cathode Material, Ferric Chloride Etching Waste, Iron Source, LiFe_0.95Mn_0.05PO₄/C

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

References

[1] C. Sun, S. Rajasekhara, J.B. Goodenough, et al. Monodisperse Porous LiFePO4 Microspheres for a High Power Li-Ion Battery Cathode[J]. Journal of the American Chemical Society, 2011, 133: 2132-2135.

DOI: 10.1021/ja1110464

Google Scholar

[2] M. Wagemaker, D.P. Singh, W.J.H. Borghols, et al. Dynamic Solubility Limits in Nanosized Olivine LiFePO4[J]. Journal of the American Chemical Society, 2011, 133: 10222-10228.

DOI: 10.1021/ja2026213

Google Scholar

[3] D. Jugovic, D. Uskokovic. A review of recent developments in the synthesis procedures of lithium iron phosphate powders[J]. Journal of Power Sources, 2009, 190(2): 538-544.

DOI: 10.1016/j.jpowsour.2009.01.074

Google Scholar

[4] D. Zhao, Y.L. Feng, Y.G. Wang, et al. Electrochemical performance comparison of LiFePO4 supported by various carbon materials[J]. Electrochimica Acta, 2013, 88: 632-638.

DOI: 10.1016/j.electacta.2012.10.101

Google Scholar

[5] M. Vujkovic, I. Stojkovic, N. Cvjeticanin, et al. Gel-combustion synthesis of LiFePO4/C composite with improved capacity retention in aerated aqueous electrolyte solution[J]. Electrochimica Acta, 2013, 92: 248-256.

DOI: 10.1016/j.electacta.2013.01.030

Google Scholar

[6] S.M. Zheng, X. Wang, X. Huang, et al. Hydrothermal synthesis of Ni-doped carbom-like LiFe0. 95Ni0. 05PO4 powders[J]. Ceramics International, 2012, 38(5): 4391-4394.

DOI: 10.1016/j.ceramint.2012.01.025

Google Scholar

[7] X.Q. Qu, G.C. Liang, J.S. Liang, et al. LiFePO4 doped with magnesium prepared by hydrothermal reaction in glucose solution[J]. Chinese Chemical Letters, 2008, 19: 345-349.

DOI: 10.1016/j.cclet.2007.10.052

Google Scholar

[8] B. Pei, Q. Wang, W. Xin, et al. Enhanced performance of LiFePO4 through hydrothermal synthesis coupled with carbon coating and cupric ion doping[J]. Electrochimica Acta, 2011, 56(16): 5667-5672.

DOI: 10.1016/j.electacta.2011.04.024

Google Scholar