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Preparation of Zirconia Nanoparticles in Ionic Liquid –Water and Characterization

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Abstract:

Zirconia nanoparticles were prepared in ionic liquid BMIMBF4-water using zirconium salt (ZrOCl2•8H2O), urea as raw material by hydrothermal synthesis method. The structure and morphology of zirconia were characterized by XRD and TEM. The experimental results showed zirconia nanoparticles could be prepared at 170°C for 24 hours in a hydrothermal kettle. Its size was about 10-30nm and the particles dispersed uniformly, and had no agglomeration phenomenon.

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Periodical:

Applied Mechanics and Materials (Volumes 52-54)

Pages:

630-632

DOI:

https://doi.org/10.4028/www.scientific.net/AMM.52-54.630

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Online since:

March 2011

Authors:

Xiang Dong Ma, Fei Lei Liu, Hui Zhang, Liu Jie Xu, Shi Zhong Wei, Ji Wen Li, Guo Shang Zhang

Keywords:

Hydrothermal Synthesis, Ionic Liquid (IL), Zirconia Nanoparticle

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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