Ultrasound-Pulse Electrodeposition Preparation of Fe-Nano ZrO₂ Functional Gradient Coating

Abstract:

Objective On the basis of the experimental investigation of Fe-ZrO₂ nanocomposite coating, nanoZrO₂ particles were added to the bath to prepare the nanocomposite coating of Fe-ZrO₂ with electroplating methods and laser cladding. Methods Study the effects of nanocontent, cathodic pulse current density, duty cycle, the ultrasonic frequency content of the coating surface Nano, orthogonal optimization of process parameters. Results The results show that nanoparticles concentration 10 g/l, the cathode current density pulse 4A/dm², the duty cycle 20%, ultrasonic frequency 180W, nanocomposite coating capacity of up to 5.5wt%. Conclusion Fe-ZrO₂ nanocomposite coating improved abrasion and Corrosion of the binary composite coating.

• Periodical: Applied Mechanics and Materials (Volumes 556-562)
• Pages: 222-227
• DOI: https://doi.org/10.4028/www.scientific.net/AMM.556-562.222
• Online since: May 2014
• Authors: Shuai Yan, Meng Hua Wu*, Zhi Ning, Yuan Gang Wang
• Keywords: Fe-ZrO₂ Nanocomposite Coating, Low-Temperature Iron Plating Coatings, Orthogonal, Ultrasound Electrodeposition

References

[1] Wang Rongguo, Wu Weili, GuWanLi. Introduction to composite materials [M]. Harbin: Harbin industrial university press, (1999).

[2] Huang Yanbin, Shao Xinhai, Song Gaowei. Research of Influencing Factors on Performance and ProcessOptimization of Ceramic Coating[J]. Equipment Environmental Engineering, 2012, 9(1): 90-93.

[3] Yu wenzhong, Yu Hongying, Sun Dongbai. Unconventional rapid electrodeposition method and principle of preparation of nanometer materials [J]. Equipment Environmental Engineering, 2007, 5(4): 78-81.

[4] Xue Jinhai, Wu Menghua, Xia Fafeng. Ultrasonic electrodeposition Ni-TiN microstructure and mechanical properties of composite coating research [J]. Journal of surface technology, 2009, 38 (4) : 4.

[5] Zhang Yingjie, Yan Yuxing, Zhang JiangHong. The advantages and disadvantages of electrodeposition of nanometer multilayer films prepared by the technology and its research progress [J]. Materials protection, 2009, 42 (8) : 5.

[6] Chen Hanbin, Zhou Jing, Wu Hulin. Duty ratio on the high frequency pulse electrodeposition (Ni, Co)/nano Al2O3 composite coating [J]. Surface Technology, 2013, 4: 56-58.

[7] Xia Fafeng, Jia Zhenyuan, Wu Menghua. Ultrasonic - base TiN electrodeposition nickel nano composite coating research [D]. Dalian: dalian university of technology, (2008).

DOI: 10.1049/cp:20060724

[8] Aogaki, R. Micro-MHD effect on electrodeposition in the vertical magnetic field[J]. Magnitnaya Gidrodinamika. 2003, 39 (4): 453-461.

[9] Chen Yuehua, Liu Yongyong Jiang Defeng. Electroless nickel plating process stability analysis [J]. Surface Technology, 2013, 2: 74-76.

[10] J. A. Koza, M. Uhlemann, A. Gebert, et al. The effect of a magnetic field on the pH value in front of the electrode surface during the electro deposition of Co, Fe and Co-Fe alloys [J]. Journal of Electro-analytical Chemistry. 2008, 617 (2): 194-202.

DOI: 10.1016/j.jelechem.2008.02.009

[11] H. Matsushima, A. spas, A. Bund, et al. Magnetic field effects on the initial stages of electro deposition processes [J]. Journal of Electro analytical Chemistry. 2008, 615 (2): 191-196.

DOI: 10.1016/j.jelechem.2007.12.010

[12] Si Donghong, Xue Yujun, Shen Chen. Ultrasonic electrodeposition of preparation of Ni-ZrO2 nanometer composite coating and its structure and performance study [J]. Journal of surface technology, 2010, 3 (39) : 10-12.

[13] Xia F F, Liu C, Wang F, et a1. Preparation and characterization of Nano Ni-TiN coatings deposited by ultrasonic electrode- position[J]. Journal of Alloys and Compounds. 2010, 490: 43l-435.

DOI: 10.1016/j.jallcom.2009.10.026

[14] Wei z J, Wang Y Want C eta1．Study of waters in nickel electroforming of 3D micro structures．Material Chemistry mad Physics, 2000, 63: 235-239.

[15] Chou M C, Yang H, Yeh S H．Micro-composite electroforming for liga technology．Micro-system Technologies, 2001, 7: 36-39.