Effect of Ultrasonic Pre-Treatment Durations on the Formation of Zeolite-T

Izzati Binti Mohamad Abdul Wahab; Yin 	Fong Yeong

doi:10.4028/www.scientific.net/AMM.625.911

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HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vol. 625Effect of Ultrasonic Pre-Treatment Durations on...

Effect of Ultrasonic Pre-Treatment Durations on the Formation of Zeolite-T

Abstract:

In the present work, the lengthy synthesis duration of zeolite-T was successfully reduced by inducing the ultrasonic pre-treatment method prior to hydrothermal growth. The effect of ultrasonic pre-treatment durations on the formation of zeolite-T was investigated. The structure and morphology of the resultant samples were characterized by FTIR, XRD and FESEM. As verified by FTIR, samples produced using synthesis durations of 5, 4, 3 and 2 days with ultrasonic pre-treatment durations of 60 min and 90 min, respectively, demonstrated zeolite-T structure. One day synthesis duration was not sufficient for the formation of zeolite-T. From the results obtained by XRD and FESEM, it was found that samples underwent 60 min ultrasonic pre-treatment produced zeolite-T with higher crystallinity, while no significant changes on the morphology of the resultant zeolite-T synthesized using ultrasonic pre-treatment durations of 60 min and 90 min.

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Periodical:

Applied Mechanics and Materials (Volume 625)

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911-915

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https://doi.org/10.4028/www.scientific.net/AMM.625.911

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Online since:

September 2014

Authors:

Izzati Binti Mohamad Abdul Wahab, Yin Fong Yeong*

Keywords:

Characterization, Crystallinity, Synthesis, Ultrasonic Pre-Treatment, Zeolite-T

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