Synthesis of Nanoporous Zinc Oxide by Anodizing of Zinc in Distilled Water

Article Preview

Abstract:

In this work, ZnO nanoporous thin films were formed by anodizing of Zn plates in 500 ml distilled water of 25°C at voltage ranged from 10 V to 30 V. As anodized zinc plates were characterized by using SEM and XRD. Characterization of as anodized Zn plates using SEM showed that the morphology of the as anodized Zn plates were significantly influenced by the anodizing voltages. Nanoporous ZnO thin films were formed when 25 V and 30 V were used while ZnO thin films without nanoporous structures were formed when 10 V, 15 V and 20 V were used. XRD analysis indicated the ZnO thin films formed at 10 V to 30 V were of hexagonal wurtzite structures.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

1126-1130

Citation:

Online since:

April 2015

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2015 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] J. Wang and L. Gao, Hydrothermal synthesis and photoluminescence properties of ZnO nanowires, Solid State Commun. 132 (2004), 269-271.

DOI: 10.1016/j.ssc.2004.07.052

Google Scholar

[2] K. S. Babu, R. A. Reddy, R. A. Sujatha and K. V. Reddy, Synthesis and optical characterization of porous ZnO, J. Adv. Ceramics. 2 (2013), 260-265.

DOI: 10.1007/s40145-013-0069-6

Google Scholar

[3] A. Sekar, S. H. Kim, A. Umar and Y. B. Hanh, Catalyst-free synthesis of ZnO nanowires on Si by oxidation of Zn powders, J. Cryst. Growth. 280 (2005), 509-515.

DOI: 10.1016/j.jcrysgro.2005.02.006

Google Scholar

[4] H. Chik, J. Liang, S. G. Cloutier, N. Kouklin and J. M. Xu, Periodic array of uniform ZnO nanorods by second-order self-assembly, Appl. Phys. Lett. 84 (2004), 3376-3378.

DOI: 10.1063/1.1728298

Google Scholar

[5] R. S. Yadav, A. C. Pandey and S.S. Sanjey, ZnO porous structures synthesized by CTAB-assisted hydrothermal process, Struct. Chem. 18 (2007), 1001-1004.

DOI: 10.1007/s11224-007-9251-1

Google Scholar

[6] D. Ramimoghadam, Mohd. Zubir Bin Hussein and Yun Hin Taufiq-Yap, The effect of sodium dodecyl sulfate (SDS) and cetyltrimethylammonium bromide (CTAB) in the properties of ZnO synthesized by hydrothermal method, Int. J. Mol. Sci. 13 (2007).

DOI: 10.3390/ijms131013275

Google Scholar

[7] L. Junwei, L. Zhifeng, E. Lei and Z. Zhichen, Effects of potential and temperature on the electrodeposited porous zinc oxide films, J. Wuhan. Univ. Technol. 26 (2011), 47-51.

DOI: 10.1007/s11595-011-0165-9

Google Scholar

[8] A. J. Yin, J. Li, W. Jian, A. J. Bennet and J. M. Xu, Fabrication of highly ordered metallic nanowire arrays by electrodeposition, Appl. Phys. Lett. 79 (2001), 1039-1041.

DOI: 10.1063/1.1389765

Google Scholar

[9] C. H. Voon, M. N. Derman, and U. Hashim, Effect of manganese content on the fabrication of porous anodic alumina, J. Nanomater. 2012 (2012), 1-9.

DOI: 10.1155/2012/752926

Google Scholar

[10] C. H. Voon, M. N. Derman, U. Hashim, K. R. Ahmad, and K. L. Foo, Effect of temperature of oxalic acid on the fabrication of porous anodic alumina from Al-Mn alloys, J. Nanomater. 2013 (2013), 1-8.

DOI: 10.1155/2013/167047

Google Scholar

[11] C.H. Voon, M.N. Derman, U. Hashim, K.R. Ahmad, and L.N. Ho, A simple one-step anodising method for the synthesis of ordered porous anodic alumina, J. Exe. Nanosci. 9 (2014), 106-112.

DOI: 10.1080/17458080.2011.630151

Google Scholar

[12] C. H. Voon, M. N. Derman, U. Hashim and K. R. Ahmad, Effect of anodizing voltage on the growth kinetics of porous anodic alumina on Al-0. 5 wt% Mn alloys, Adv. Mat. Res. 795 (2013), 56-59.

DOI: 10.4028/www.scientific.net/amr.795.56

Google Scholar

[13] C. H. Voon, M. N. Derman, U. Hashim, and K. L. Foo and T. Adam, Effect of anodizing voltage on the morphology and growth kinetics of porous anodic alumina on Al-0. 5 wt% Mn alloys, Adv. Mat. Res. 832 (2014), 101-106.

DOI: 10.4028/www.scientific.net/amr.832.101

Google Scholar

[14] L. S. Chuah, Z. Hassan and S. K. Mohd Bakhori, Nanoporous ZnO prepared by electrochemical anodization deposition, Third International Conference on Smart Materials and Nanotechnology in Engineering, Malaysia. 8409 (2011), 84092E-1 – 84092E-6.

DOI: 10.1117/12.916627

Google Scholar

[15] Y. Yamaguchi, M. Yamazaki, S. Yoshihara and T. Shirakashi, Photocatalytic ZnO films prepared by anodizing, J. Electroanal. Chem. 442 (1998), 1-3.

DOI: 10.1016/s0022-0728(97)00354-9

Google Scholar

[16] S. W. Ng, F. K. Yam, L. L. Low, K. P. Beh, M. F. Muatapha, E. N. Sota, S. S. Tneh and Z. Hassan, Self-assembled ZnO nanostripes prepared by acidified ethanolic anodization, Optoelectron. Adv. Mat. 5(2011), 89-91.

Google Scholar

[17] A. Ravanbakshah, F. Rashni, M. H. Sohi and R. K. Nekoui, Synthesis of nanostructured zinc oxide thin films by anodic oxidation, Adv. Mater. Res. 839 (2013), 347-351.

DOI: 10.4028/www.scientific.net/amr.829.347

Google Scholar

[18] S. Amitha and N. K. Karuna, Synthesis of zinc oxide porous structures by anodization with water as electrolyte, Appl. Phys. A. 129 (2012), 151-157.

Google Scholar