Preparation and Optical Properties of Er3+-Yb3+ Co-Doped ZnO-B2O3- SiO2 -TiO2Transparent Glass-Ceramics

Qin Lei Wei; Xiang Yu Zou; Hong Bo Zhang; Chun Hui Su

doi:10.4028/www.scientific.net/AMR.1004-1005.330

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 1004-1005Preparation and Optical Properties of Er3+-Yb3+...

Preparation and Optical Properties of Er³⁺-Yb³⁺ Co-Doped ZnO-B₂O₃- SiO₂-TiO₂Transparent Glass-Ceramics

Abstract:

Er³⁺-Yb³⁺co-doped ZnO-B₂O₃- SiO₂-TiO₂ transparent glass ceramics were synthesized by melt crystallization technique. Samples were characterized by DSC, XRD, SEM, UV-Vis-NIR and fluorescence spectra and the factors affecting the crystallization of glass ceramics were analyzed. The results indicated good crystallization property of ZBS glass ceramics. The optimum crystallization temperature was 800°C, and crystallization time was 60 min. The main crystal phase was Zn₂TiO₄ and the transmittance was up to 70% in visible light region. SEM micrograph indicated that the grain diameter was less than 100nm and the emission spectrum of glass ceramics displayed by fluorescence spectra was greatly improved compared with matrix glass. Strong emission peak was observed at 1535nm.

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Periodical:

Advanced Materials Research (Volumes 1004-1005)

Pages:

330-334

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1004-1005.330

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Online since:

August 2014

Authors:

Qin Lei Wei, Xiang Yu Zou, Hong Bo Zhang*, Chun Hui Su

Keywords:

Er³⁺-Yb³⁺ Co-Doped, Glass-Ceramics, ZnO-B₂O₃- SiO₂-TiO

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