Paper Titles

An Unexpected Synthesis of 2H-Benzimidazole Derivatives
p.43

Synthesis of an Akt Inhibitor-IV Analogue via an Amine-Exchange Reaction
p.47

An H-Phosphonate Approach for the Preparation of Purine-Nucleoside Monophosphates
p.51

Synthesis of Symmetrical Dipurine-Nucleoside Diphosphates from the Corresponding Nucleoside Phosphoropiperidates
p.55

Preparation of Modified 1,6-Hexanediamines
p.59

Synthesis of Guanosine-Containing Dinucleoside Triphosphates
p.63

Sustained Release Properties of Aminophylline Sustained Release Tablets Based on Exfoliated Graphite
p.67

Research on Allelochemicals with Material Properties Exuded by Submerged Freshwater Macrophyte Elodea nuttallii
p.71

Synthesis of P¹, P³-Distavudine-5′, 5′-Triphosphate
p.75

HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 1023Preparation of Modified 1,6-Hexanediamines

Preparation of Modified 1,6-Hexanediamines

Article Preview

Abstract:

A series of novel 1,6-diaminohexanes functionalized with phosphonates have been synthesized under solvent-free conditions and characterized by NMR and MS. The experimental results indicated that excess aldehyde and phosphite and elevated temperature were required for effective formation of the bis-funcationalized alkyl diamines.

You might also be interested in these eBooks

Advanced Research on Energy, Chemistry, Materials and Informatization III

Info:

Periodical:

Advanced Materials Research (Volume 1023)

Pages:

59-62

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1023.59

Citation:

Cite this paper

Online since:

August 2014

Authors:

Xiao Chuan Li, Shan Shan Gong, Qi Sun*

Keywords:

Diamine, Imine, Kabachnik-Fields Reaction, Phosphonate, Solvent-Free

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] R.A. Smiley, in: Ullmann's Encyclopedia of Industrial Chemistry. Hexamethylenediamine. Wiley-VCH, Weinheim, (2005).

[2] G. Prömpers, H. Keul, H. Höcker, Des. Monomers and Polym. Vol. 8 (2005), p.547.

[3] R.J. Palmer, in: Encyclopedia of Polymer Science and Technology. Polyamides, Plastics, John Wiley & Sons, Inc, (2001).

[4] L. Ubaghs, N. Fricke, H. Keul, H. Höcker, Macromol. Rapid Commun. Vol. 25 (2004), p.517.

DOI: 10.1002/marc.200300064

[5] S. Failla, P. Flnocchiaro, G.L. Rose, Phosphorus, Sulfur and Silicon Vol. 113 (1996), p.225.

[6] J. Lewkowski, P. Tokarz, T. Lis, K. Slepokura, Tetrahedron. Vol. 70 (2014), 810.

[7] J. Lewkowski, P. Tokarz, T. Lis, K. Slepokura, Tetrahedron Asymmetry Vol. 23 (2012), p.482.

[8] P. Hamm, US Patent Vol. 3 (1971), p.556.

[9] A. Hille, R. Gust, Arch. Pharm. Chem. Life Sci. Vol. 342 (2009), p.625.

[10] S. Bhagat, A.K. Chakraborti, J. Org. Chem. Vol. 72 (2007), p.1263.

[11] J. Wu, W. Sun, H. Xia, X. Sun, Org. Biomo. Chem. Vol. 4 (2006), p.1663.

[12] X. Mu, M. Lei, J. Zou, W. Zhang, Tetrahedron Lett. Vol. 47 (2006), p.1125.

[13] K. Manabe, S. Kobayashi, Chem. Commun. Vol. (2000), p.669.

[14] T. Akiyama, M. Sanada, K. Fuchibe, Synlett, (2003), p.1463.

[15] G.D. Joly, E.N. Jacobsen, J. Am. Chem. Soc. Vol. 126 (2004), p.4102.

[16] A. Heydari, A. Javidan, M. Shaffie, Tetrahedron Lett. Vol. 42 (2001), p.8071.