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Effect of Applied Voltage on the Formation of Self-Organized Iron Oxide Nanoporous Film in Organic Electrolyte via Anodic Oxidation Process and their Photocurrent Performance
Abstract:
Anodisation of iron foil was done to produce anodic film with nanoporous structure. The effect of anodic voltage on the morphology of the anodic oxide formed was investigated. Anodic film formed on iron foil anodised at 10 V is rather compact no obvious pores. Pores can be detected on oxide anodised at 30 V despite not very uniform. For foil anodised at 50 V, 1.8 µm thick anodic layer which consisted of uniform circular pores is observed. This film was then annealed at 450°C for 3 h in air as to induce crystallinity. The annealed nanoporous film exhibits a light illuminated photocurrent of 0.45 mA in 1 M NaOH + H2O2 solution.
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99-103
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Online since:
August 2014
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© 2014 Trans Tech Publications Ltd. All Rights Reserved
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