Alloying of Molybdenum Disilicide with Aluminum by SHS

Article Preview

Abstract:

In this work, a series of samples of Mo (Si1-xAlx)2 (X =0, 0.10,0.20,0.30,0.40) were prepared by self-propagating high-temperature synthesis (SHS). The influence of the addition of Al on the structures and the micrographs of the final compounds were investigated. X-ray diffraction pattern characterization (XRD) and scanning electron microscopy (SEM) were used to characterize the obtained products. It was found that, the reactions between Mo and Si could be promoted with introducing Al during the SHS process. The high temperature β-MoSi2 phase with hexagonal structure (C40) was obtained and the peaks of the C40 phase shifted towards a higher d value with increasing aluminum substitution. The substitution of Al could reach to 40%. The morphology of the final products was similar with that of the raw Mo powders, which was independent of Al contents.

You might also be interested in these eBooks

Info:

Periodical:

Advanced Materials Research (Volumes 1025-1026)

Pages:

585-590

Citation:

Online since:

September 2014

Keywords:

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] A. Chrysanthou, R.C. Jenkins, M.J. Whiting, et al: J. Mater. Sci. Vol. 31 (1996), p.4221.

Google Scholar

[2] J.N. Woolman, J.J. Petrovic, Z.A. Munir: J. Mater. Sci. Vol. 39 (2004), p.5037.

Google Scholar

[3] L. Ingemarsson, K. Hellstro¨m, S. Canovic, et al: J. Mater. Sci. Vol. 48 (2013), p.1511.

Google Scholar

[4] Raghavan V. Al-Mo-Si (Aluminum-Molybdenum-Silicon). J. Phase Equilib Diff. Vol. 33 (2012), p.329.

DOI: 10.1007/s11669-012-0069-1

Google Scholar

[5] Y. Qiao, H. Zhang, C. Hong, et al: J. Phys. Appl. Phys. Vol. 42 (2009), p.1.

Google Scholar

[6] M. Lynda, M. Benoıˆt, C. Marle`ne, et al: J. Mater. Sci. Vol. 47 (2012), p.6792.

Google Scholar

[7] A. Stergiou, P. Tsakiropoulos, A. Brown: Intermetallics Vol. 5, No. 1 (1997), p.69.

Google Scholar

[8] S. Hasani, M. Panjepour, M.A. Shamanian: J. Alloy Compd. Vol. 502 (2010), p.80.

Google Scholar

[9] M. Lynda, M. Benoit, Marlene, et al: J. Mater. Sci. Vol. 47 (2012), p.6792.

Google Scholar

[10] Y. Zhou, C. Wei, Ye Guotian, et al: The Effects of Particle Size and Morphology of Raw Materials on the Properties of MoSi2 Synthesized by SHS[C]. /Chemical, Mechanical and Materials EngineeringⅡ, Melbourne, Australia, Vol. 319 (2013), p.213.

DOI: 10.4028/www.scientific.net/amm.319.213

Google Scholar

[11] S.C. Deevi: Int. J. Refract Met. Hard Mater. Vol. 13 (1995), p.337.

Google Scholar

[12] S.W. Jo, G.W. Lee, J.T. Moon, et al: J. Acta. Mater. Vol. 44 (1996), p.4317.

Google Scholar