Graphene Oxide-Reinforced Hollow Fiber Solid-Phase Microextraction Coupled with HPLC for the Determination of Parabens in Beer

Ting Gao; Neng Sheng Ye

doi:10.4028/www.scientific.net/AMR.1033-1034.544

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 1033-1034Graphene Oxide-Reinforced Hollow Fiber Solid-Phase...

Graphene Oxide-Reinforced Hollow Fiber Solid-Phase Microextraction Coupled with HPLC for the Determination of Parabens in Beer

Abstract:

An effective and sensitive method to determinate four parabens was developed by using graphene oxide (GO)-reinforced hollow fiber (HF) solid-phase microextraction combined with HPLC-PDA. Scanning electron microscope characterizations indicated that graphene oxide was successfully synthesized and modified in the pores of HF by ultrasonication. The conditions including extraction time, desorption time were optimized. The liner ranges of parabens were 0.01-5.00 μg/mL via the proposed management with a limitation of detection of 0.005 μg/mL. The extraction procedure based on GO-HF was successfully used for the determination of parabens in beer.

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Periodical:

Advanced Materials Research (Volumes 1033-1034)

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544-547

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https://doi.org/10.4028/www.scientific.net/AMR.1033-1034.544

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Online since:

October 2014

Authors:

Ting Gao, Neng Sheng Ye*

Keywords:

Graphene, Hollow Fiber, Parabens, Solid-Phase Microextraction

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References

[1] S. Wu, Q. He, C. Tan, Y. Wang, H. Zhang, Graphene-Based Electrochemical Sensors, Small 9 (2013) 1160-1172.

DOI: 10.1002/smll.201202896

Google Scholar

[2] Y. Liu, X. Dong, P. Chen, Biological and chemical sensors based on graphene materials, Chem. Soc. Rev. 41 (2012) 2283-2307.

DOI: 10.1039/c1cs15270j

Google Scholar

[3] J. Tian, J. Xu, F. Zhu, T. Lu, C. Su, G. Ouyang, Application of nanomaterials in sample preparation, J. Chromatogr. A 1300 (2013) 2-16.

Google Scholar

[4] B. Zhang, X. Zheng, H. Li, J. Lin, Application of carbon-based nanomaterials in sample preparation: A review, Anal. Chem. Acta 784 (2013) 1-17.

Google Scholar

[5] N.S. Ye, P.Z. Shi, J. Li, Q. Wang, Application of graphene as solid phase extraction absorbent for the determination of parabens in cosmetic products by capillary electrophoresis, Anal. Lett. 46 (2013) 1991-(2000).

DOI: 10.1080/00032719.2013.784916

Google Scholar

[6] N.S. Ye, P.Z. Shi, Q. Wang, J. Li, Graphene as solid-phase extraction adsorbent for CZE determination of sulfonamide residues in meat samples, Chromatographia 76 (2013) 553-557.

DOI: 10.1007/s10337-013-2394-x

Google Scholar

[7] M.D. Stoller, S.J. Park, Y.W. Zhu, J.H. An, R.S. Ruoff, Graphene-based ultracapacitors, Nano Lett. 8 (2008) 3498-3502.

DOI: 10.1021/nl802558y

Google Scholar

[8] Y. Cai, G. Jiang, J. Liu, Q. Zhou, Multiwalled carbon nanotubes as a solid-phase extraction adsorbent for the determination of bisphenol A, 4-n-nonylphenol, and 4-tert-octylphenol, Anal. Chem. 75 (2003) 2517-2521.

DOI: 10.1021/ac0263566

Google Scholar

[9] Y. Yang, J. Chen, Y.P. Shi, Determination of diethylstilbestrol in milk using carbon nanotube-reinforced hollow fiber solid-phase microextraction combined with high-performance liquid chromatography, Talanta 97 (2012) 222-228.

DOI: 10.1016/j.talanta.2012.04.021

Google Scholar

[10] X.Y. Song, Y.P. Shi, J. Chen, A novel extraction technique based on carbon nanotubes reinforced hollow fiber solid/liquid microextraction for the measurement of piroxicam and diclofenac combined with high performance liquid chromatography, Talanta 100 (2012).

DOI: 10.1016/j.talanta.2012.08.042

Google Scholar

[11] X.Y. Song, Y.P. Shi, J. Chen, Carbon nanotubes-reinforced hollow fibre solid-phase microextraction coupled with high performance liquid chromatography for the determination of carbamate pesticides in apples, Food Chem. 139 (2013) 246-252.

DOI: 10.1016/j.foodchem.2013.01.112

Google Scholar

[12] M.H. Liu, B. Qiu, X. Jin, L. Zhang, X. Chen, G.N. Chen, Determination of estrogens in wastewater using three-phase hollow fiber-mediated liquid-phase microextraction followed by HPLC, J. Sep. Sci. 31 (2008) 622-628.

DOI: 10.1002/jssc.200700497

Google Scholar

[13] D.A. Lambropoulou, T.A. Albanis, Application of hollow fiber liquid phase microextraction for the determination of insecticides in water, J. Chromatogr. A 1072 (2005) 55-61.

DOI: 10.1016/j.chroma.2004.11.076

Google Scholar

[14] S.W. Su, B.B. Chen, M. He, B. Hu, Graphene oxide-silica composite coating hollow fiber solid phase microextraction online coupled with inductively coupled plasma mass spectrometry for the determination of trace heavy metals in environmental water samples, Talanta 123 (2014).

DOI: 10.1016/j.talanta.2014.01.061

Google Scholar