Preparation of Hollow Nickel Ferrite Microspheres and their Magnetic Properties

Article Preview

Abstract:

Hollow nickel ferrite microspheres with a diameter of about 1.5 to 2.5 μm were synthesized using an emulsion-based solvothermal method in combination with calcination at 550°C. The structures and morphologies of the nickel ferrite microspheres were characterized using an X-ray diffractometer, a transmission electron microscopy and a field emission scanning electron microscopy. Magnetization measurement was carried out using a vibrating sample magnetometer at room temperature. The saturation magnetization and coercivity of nickel ferrite microspheres could reach 19.41 emu/g and 202.28 Oe, respectively. Hollow nickel ferrite microspheres might be used as catalysts, magnetic materials and microwave absorbers.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

488-491

Citation:

Online since:

October 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] S. Chikazumi, S. Taketomi, M. Ukita, M. Mizukami, H. Miyajima, M. Setogawa, Y. Kurihara, J. Magn. Magn. Mater. 3 (1987) 907-914.

Google Scholar

[2] Y. W. Jun, Y. M. Huh, J. S. Choi, J. H. Lee, H. T. Song, S. Kim, S. Yoon, K. S. Kim, J. Shin, S. Cheon, J. Am. Chem. Soc. 127 (2005) 5732-5733.

DOI: 10.1021/ja0422155

Google Scholar

[3] R. C. Che, L. M. Peng, X. F. Duan, Q. Chen, X. L. Liang, Adv. Mater. 16 (2004) 401-405.

Google Scholar

[4] D. Chiba, M. Sawicki, Y. Nishitani, Y. Nakatani, F. Matsukur, H. Ohno, Nature 455 (2008) 515-518.

DOI: 10.1038/nature07318

Google Scholar

[5] Z. Li, L. Wei, M. Y. Gao, H. Lei, Adv. Mater. 17 (2005) 1001-1005.

Google Scholar

[6] S. W. Cao, Y. J. Zhu, J. Phys. Chem. C 112 (2008) 12149-12156.

Google Scholar

[7] C. R. Gong, D. R. Chen, X. L. Jiao, Q. L. Wang, J. Mater. Chem. 12 (2002) 1844-1847.

Google Scholar

[8] Q. Dong, N. Kumada, Y. Yonesaki, N. Kinomura, D. Wang, J. Mater. Sci. 45 (2010) 5685-5691.

Google Scholar

[9] J. Ming, Y. Q. Wu, L. Y. Wang L, J. Mater. Chem. 21 (2011) 17776-17782.

Google Scholar

[10] M. Fu, Q. Z. Jiao, Y. Zhao and H. S. Li, J. Mater. Chem. A 2 (2014) 735-744.

Google Scholar

[11] Y. D. Meng, D. R. Chen and X. L. Jiao, Eur. J. Inorg. Chem. 20 (2008) 4019-4023.

Google Scholar

[12] J. Eastoe, S. Gold, S. E. Rogers, A. Paul, T. Welton, R. K. Heenan, I. Grillo, J. Am. Chem. Soc. 127 (2005) 7302-7303.

DOI: 10.1021/ja051155f

Google Scholar