Production and Quality Assessment of Superelastic Ti-Nb-Based Alloys for Medical Application

Article Preview

Abstract:

Superelastic biocompatible metallic materials Ti-22Nb-6Zr and Ti-22Nb-3Ta-3Zr (at %) were produced. Vacuum arc remelting (VAR) with manual control allowed to produce high‑purity alloys. X-ray fluorescence spectrometry (XRF) results showed that one remelt was not enough to obtain homogeneous Ti-Nb-Ta-Zr ingot. Ti-Nb-Zr and Ti-Nb-Ta-Zr alloys were remelted 3 times and turned upside down after each remelting. Scanning electron microscopy (SEM) with micro X‑ray spectral analysis showed that chemical composition of the alloys coincided with nominal chemical composition. SEM results also showed that the alloys were mostly homogeneous. Recommendations for optimization of VAR in terms of producing high-purity homogeneous superelastic titanium alloys were elaborated.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

130-136

Citation:

Online since:

September 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Hee Young Kim, Yoshinori Ohmatsu, Jae Il Kim, Hideki Hosoda and Shuichi Miyazaki, Mechanical Properties and Shape Memory Behavior of Ti-Mo-Ga Alloys, Materials Transactions , 45, 4 (2004) 1090-1095.

DOI: 10.2320/matertrans.45.1090

Google Scholar

[2] Takashi Maeshima and Minoru Nishida, Shape Memory Properties of Biomedical Ti-Mo-Ag and Ti-Mo-Sn Alloys, Materials Transactions, 45, 4 ( 2004) 1096-1100.

DOI: 10.2320/matertrans.45.1096

Google Scholar

[3] Eiji Takahashi, Tasuku Sakurai, Sadao Watanabe, Naoya Masahashi and Shuji Hanada, Effect of Heat Treatment and Sn Content on Superelasticity in Biocompatible TiNbSn Alloys, Materials Transactions, 43, 12 (2002) 2978-2983.

DOI: 10.2320/matertrans.43.2978

Google Scholar

[4] M. Tahara, H.Y. Kim, H. Hosoda, S. Miyazaki Cyclic deformation behavior of a Ti–26 at. % Nb alloy, Acta Materialia 57 (2009) 2461-2469.

DOI: 10.1016/j.actamat.2009.01.037

Google Scholar

[5] L. W. Ma, H. S. Cheng, C. Y. Chung Effect of thermo-mechanical treatment on superelastic behavior of Ti–19Nb–14Zr (at. %) shape memory alloy, Intermetallics, 32 (2013) 44-50.

DOI: 10.1016/j.intermet.2012.07.024

Google Scholar

[6] Masaki Tahara, Hee Young Kim, Hideki Hosoda, Tae-hyun Nam, Shuichi Miyazaki Effect of nitrogen addition and annealing temperature on superelastic properties of Ti-Nb-Zr-Ta alloys, Materials Science and Engineering: A, 527 (2010) 6844-6852.

DOI: 10.1016/j.msea.2010.07.052

Google Scholar

[7] Li Nie, Yongzhong Zhan, Tong Hu, Xiaoxian Chen, Chenghui Wang, β-Type Zr–Nb–Ti biomedical materials with high plasticity and low modulus for hard tissue replacements, Journal of the Mechanical Behavior of Biomedical Materials, 29 (2014) 1-6.

DOI: 10.1016/j.jmbbm.2013.08.019

Google Scholar

[8] Qianqian Weia, Liqiang Wanga, Yuanfei Fub, Jining Qina, Weijie Lua, Di Zhanga, Influence of oxygen content on microstructure and mechanical properties of Ti–Nb–Ta–Zr alloy, Materials & Design, 32, (2011) 2934-2939.

DOI: 10.1016/j.matdes.2010.11.049

Google Scholar