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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 1120-1121Microwave Synthesis of the Composites...

Microwave Synthesis of the Composites (α-Al₂O₃+TiB₂)/NiAl from Al-TiO-B-Ni System

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Abstract:

NiAl matrix composites reinforced with a-Al2O3 and TiB2 were fabricated by microwave synthesis from Al-TiO2-B-Ni system. The reaction process and microstructures were analyzed by using differential scanning calorimetry (DSC), X-ray diffraction (XRD), scanning electron microscopy (SEM).The results showed that the ignition temperatures of the reaction heating by microwave and conventional method were approximately 556°C and 592°C respectively. Furthermore, the fabrication time by microwave synthesis was about several minutes, which was much shorter than two hours spent usually in conventional heating method. The a-Al2O3 phase aggregated at the trigonal grain boundary of the NiAl matrix, and the TiB2 phase distributed uniformly in the NiAl matrix.

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Periodical:

Advanced Materials Research (Volumes 1120-1121)

Pages:

604-607

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1120-1121.604

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Online since:

July 2015

Authors:

Guan Hong Guo, He Guo Zhu*

Keywords:

Differential Scanning Calorimetry (DSC), Energy Dispersive Spectroscopy (EDS), Microwave Synthesis, NiAl Matrix Composite

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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