Eutectic Microbonding of Composite Materials Using Microwave Technology

Abstract:

The paper aims to report researches in microbonding process of composite magnetic materials using as thermal source the heat produced in base materials by the conversion of the electromagnetic waves with high frequency into thermal energy. This technology can be applied by targeting the base materials with microwaves and taking into account that composite magnetic materials based on ferrites, present good absorbance and conversion properties of the microwaves into heat. For experimental research, the base materials were sintered sampled of raw products obtained from stoichiometric mixtures of 6Fe₂O₃ + BaCO₃. The raw products were obtained by milling and alloying processes using planetary ball mills. The milling and alloying processes have been perfomed in dry environement for homogeneous mixtures and wet environment for mixtures obtained using mechanical alloying. In terms of eutectic alloys used for microbonding, there have been used lead free Sn96,5%+Ag3%+Cu0,5% with melting point around 217⁰ C. The microbonding process have been perfomed in two steps: first step was focused on prepairing the base materials by cleaning and deposition of eutectic alloys on their surfaces; the second step was the heating of the base materials in microwave field. A microwave generator with adjustable input power from 0 W to 6000 W with a WR340 waveguide have been used as thermal sources. The researches have shown that the base materials were bonded using less than 10 % of microwave power and the eutectic alloys reached the melting temperature în less than 3 seconds when the magnetron was set to full power. A matching load impedance automatic tuner up to 6000 W have been used for increasing the level of absorbed power from nicrowave generator to samples and decreasing the level of rejected power from composite magnetic material to microwave generator. The temperature have been measured using IR pyrometers with range measurement between 0 and 700⁰ C. The process can be succesfully applied to a large scale for small parts of electrical engines with permanent cermic magnets.

• Periodical: Advanced Materials Research (Volume 1164)
• Pages: 17-23
• DOI: https://doi.org/10.4028/www.scientific.net/AMR.1164.17
• Online since: June 2021
• Authors: Robert Cristian Marin*, Iulian Ştefan, Răzvan Ionuţ Iacobici, Sorin Vasile Savu
• Keywords: Eutectic Microbonding, Microwave Heating Mechanism

References

[1] A.C. Metaxas, R.J. Meredith, Industrial microwave heating, IEE, (1993).

[2] Mangra, M., Ciupitu, I., Gingu, O., Savu, I.D., Savu, S.V., Bica, I., Morjan, I., Kappel, W., Dehelean, D., Processes of elaboration of nanometric and nanostructured powders, Editura Universitaria, (2008).

[3] Savu S.V., Procesarea materialelor in camp de microunde, Editura Universitaria (2013).

[4] Mangra G., Savu S.V., Savu, I.D., Inductive sensor with sintered magnetic core to evaluate the performances of the table tennis players, Materials Science Forum (2011), 105-108.

DOI: 10.4028/www.scientific.net/msf.672.105

[5] DongFengQingqingWangDaweiXuPengjuLiu, Microwave assisted sinter molding of polyetherimide/carbon nanotubes composites with segregated structure for high-performance EMI shielding applications, Composites Science and Technology Volume 182, 29 September 2019, 107753.

DOI: 10.1016/j.compscitech.2019.107753

[6] Yingguang Li, Libing Cheng & Jing Zhou, Curing multidirectional carbon fiber reinforced polymer composites with indirect microwave heating, The International Journal of Advanced Manufacturing Technology volume 97, pages1137–1147(2018).

DOI: 10.1007/s00170-018-1974-1

[7] Kamble, D. L., Kumar Sahu, R., Narendranath, S., & Badiger, R. I. (2020). Effect of input power and interfacial powder size on microwave joining of different materials: A review. Materials Today: Proceedings.

DOI: 10.1016/j.matpr.2020.07.351

[8] Qu, B., Zhuo, D., Wang, R., Wu, L., & Cheng, X. (2018). Enhancement of mechanical properties of buckypapers/polyethylene composites by microwave irradiation. Composites Science and Technology, 164, 313–318.

DOI: 10.1016/j.compscitech.2018.06.002

[9] Singh, M. K., & Zafar, S. (2018). Influence of microwave power on mechanical properties of microwave-cured polyethylene/coir composites. Journal of Natural Fibers, 1–16.

DOI: 10.1080/15440478.2018.1534192

[10] Barasinski, A., Tertrais, H., Bechtel, S., & Chinesta, F. (2018). Microwave heating for thermoplastic composites - Could the technology be used for welding applications?.

DOI: 10.1063/1.5034804