Effect of Silk Fibroin on the Properties of Calcium Phosphate Cement

Article Preview

Abstract:

To improve the physicochemical properties of calcium phosphate cement (CPC), silk fibroin (SF) in the different forms were added into CPC. The structure of the composites was studied by X-ray diffraction. The setting time was investigated by ISO Cement Standard Consistency Instrument. Scanning Electron Microscope was used to observe the surface morphology. Mechanical properties of samples were tested by Instron Universal Testing Machine. The results indicated that acicular crystal of hydroxyapatite (HA) was formed in the hardening body of both CPC with SF and the pure CPC. Addition of SF had no significant effect on the structure of SF/CPC composite. The setting time of CPC with SF was significantly shorter than that of the pure CPC (30.3 mins). The setting time of CPC by adding silk fibroin powder I (SFP) and silk fibroin fiber (SFF) was greatly shortened, which was only 11.7 minutes. The setting time of CPC with SFP decreased approximately by 1/3, while the setting time of the CPC with SFF decreased nearly by 1/2. With the adding of SF, the compressive strength of CPC increased significantly. There was a distinct increase in the work-of-compressive of CPC with the adding of SFF.

You might also be interested in these eBooks

Info:

Periodical:

Advanced Materials Research (Volumes 175-176)

Pages:

100-104

Citation:

Online since:

January 2011

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2011 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] W. E. Brown, L. C. Chow: Journal of the American Ceramic Society Vol. 69 (1986), p.352.

Google Scholar

[2] C. Niedhart, U. Maus and E. Redmann: J. Biomed. Mater. Res. Vol. 55 (2001), p.530.

Google Scholar

[3] E. M. Ooms, J. G. C. Wolke and M. T. van de Heuvel: Biomaterials Vol. 24(2003), p.989.

Google Scholar

[4] H. H. K. Xu, F. C. Eichmiller and A. A. Giuseppetti: J. Biomed. Mater. Res. Vol. 52 (2000), p.107.

Google Scholar

[5] H. H. K. Xu, F. C. Eichmiller and P. R. Barndt: Journal of Materials Science-Materials in Medicine Vol. 12 (2001), p.57.

Google Scholar

[6] H. H.K. Xu, C. G. Simon Jr: Biomaterials Vol. 26 (2005), p.1337.

Google Scholar

[7] G. H. Altman, F. Diaz and C. Jakuba: Biomaterials Vol. 24 (2003), p.401.

Google Scholar

[8] R. E. Unger, W. Michael and P. Kirsten: Biomaterials Vol. 25(2004), p.1069.

Google Scholar

[9] B. M. Min, L. Jeong and Y.S. Nam: Int. J. Biol. Macromol. Vol. 34 (2004), p.223.

Google Scholar

[10] B. M. Min, L. Jeong and Y.S. Nam: Biomaterials Vol . 25 (2004), p.1289.

Google Scholar

[11] Y. Z. Wang, U.J. Kim and D.J. Blasioli: Biomaterials Vol. 26 (2005), p.7082.

Google Scholar

[12] R. J. Xie, Q. M. Deng and H. Z. Zhan: Journal of Textile Research Vol. 30 (2009), p.5.

Google Scholar

[13] A. Cherng, S. Takagi and L.C. Chow: J. Biomed. Mater. Res. Vol. 35 (1997), p.273.

Google Scholar

[14] H. H. K. Xu, S. Takagi and J. B. Quinn, et al: J. Biomed. Mater. Res. Vol. 68A (2004), p.725.

Google Scholar

[15] L. E. Carey, H. H. K. Xu and C. G. Simon Jr, et al: Biomaterials Vol. 26(2005), p.5002.

Google Scholar

[16] C. F. Xiao: Fiber composites-fiber, matrix and mechanical properties (China Petrochemical Press, Beijing 1991).

Google Scholar

[17] Z. L. Gu: Mechanics of short fiber composite materials (National Defense Industry Press, Beijing 1987).

Google Scholar