Effect of Pressures on the Chemical Vapor Deposition of BN Using Borazine

Article Preview

Abstract:

Boron nitride coatings have been prepared by chemical vapor deposition using borazine as single precursor at 900 °C. The effect of the total pressure on the surface morphologies of the coatings was investigated. For low total pressures (≤ 3 kPa), the deposits presents a compact pebble-like surface structure. However, when high total pressures (> 3 kPa) were used, the surface of the coatings presents a loose grain-like feature. When the total pressure increases up to 12 kPa, the coatings shows a porous surface structure. The composition and structure of the deposited coatings were investigated by means of FTIR and XRD analysis. It shows that the coatings have a structure of turbostratic boron nitride.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

588-592

Citation:

Online since:

February 2011

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2011 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] R.R. Naslain, R.J.F. Pailler, J.L. Lamon: Int. J. Appl. Ceram. Technol. Vol. 7 (2010), p.263.

Google Scholar

[2] J. Eichler, C. Lesniak: J. Eur. Ceram. Soc. Vol. 28 (2008), p.1105.

Google Scholar

[3] S. Seghi, J. Lee, J. Economy: Carbon Vol. 43 (2005), p. (2035).

Google Scholar

[4] T. Uğurlu, M. Turkoğlu: Int. J. Pharm. Vol. 353 (2008), p.45.

Google Scholar

[5] S. Jacques, H. Vincent, C. Vincent, A. Lopez-Marure, J. Bouix: J. Solid State Chem. Vol. 162 (2001), p.358.

DOI: 10.1006/jssc.2001.9387

Google Scholar

[6] J. Huang, C. Pan, D. Lii: Surf. Coat. Technol. Vol. 122 (1999), p.166.

Google Scholar

[7] B. Choi: Mater. Res. Bull. Vol. 34 (1999), p.2215.

Google Scholar

[8] H. Strakov, G. Hackl, N. Popovska, H. Gerhard, C.L. Aardahl: Chem. Vapor. Depos. Vol. 10 (2004), p.325.

Google Scholar

[9] C. Lorrette, P. Weisbecker, S. Jacques, R. Pailler, J.M. Goyhénèche: J. Eur. Ceram. Soc. Vol. 27 (2007), p.2737.

Google Scholar

[10] B. Deb, B. Bhattacharjee, A. Ganguli, S. Chaudhuri, A.K. Pal: Mater. Chem. Phys. Vol. 76 (2002), p.130.

Google Scholar

[11] W. Schmolla, H.L. Hartnagel: Solid State Electron. Vol. 26 (1983), p.931.

Google Scholar

[12] S. Seghi, J. Lee, J. Economy: Carbon Vol. 43 (2005), p. (2035).

Google Scholar

[13] J. Li, C. Zhang, B. Li, F. Cao, S. Wang: Eur. J. Inorg. Chem. Vol. 2010 (2010), p.1763.

Google Scholar

[14] C. Weissmantel, K. Bewilogua, D. Dietrich, H.J. Erler, H.J. Hinneberg, S. Klose, W. Nowick, G. Reisse: Thin Solid Films Vol. 72 (1980), p.19.

DOI: 10.1016/0040-6090(80)90554-4

Google Scholar

[15] T.P. Smirnova, L.V. Jakovkina, I.L. Jashkin, N.P. Sysoeva, J.I. Amosov: Thin Solid Films Vol. 237 (1994), p.32.

DOI: 10.1016/0040-6090(94)90235-6

Google Scholar

[16] B. Li, C. Zhang, F. Cao, S. Wang, Y. Jiang: J. Inorg. Mater. Vol. 23 (2008), p.229.

Google Scholar

[17] S. Alkoy, C. Toy, T. Gönül, A. Tekin: J. Eur. Ceram. Soc. Vol. 17 (1997), p.1415.

Google Scholar