Two Steps Synthesis of Quaternary Metal Titanate of Ba2NiTi5O13 and Characterization

Yin Chew Ker; Abu Bakar Mohamad

doi:10.4028/www.scientific.net/AMR.364.353

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 364Two Steps Synthesis of Quaternary Metal Titanate...

Two Steps Synthesis of Quaternary Metal Titanate of Ba₂NiTi₅O₁₃ and Characterization

Abstract:

Quaternary metal oxide of Ba₂NiTi₅O₁₃ was synthesized by using two-step sol-gel method. Excess of titanium dioxide obtained from the first step of sol-gel synthesis, were subsequently reacted in second step of sol-gel synthesis in order to produce Ba₂NiTi₅O₁₃ monoclinic phase. Calcination temperature of 900 °C for as long as 8 hours was needed for obtaining pure phase of Ba₂NiTi₅O₁₃. Homogenous micron sized particles of Ba₂NiTi₅O₁₃ with average size of 0.10 μm and narrow distribution were observed using Scanning Electron Microscopy (SEM). Besides, porous structures can also be seen distributed across the surface of the particles of Ba₂NiTi₅O₁₃ particles. Characterization of monoclinic phase of Ba₂NiTi₅O₁₃ was described based on the investigations of X-Ray Diffraction (XRD), Fourier Transform Infrared (FTIR) and Thermo Gravimetric Analysis (TGA).

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Periodical:

Advanced Materials Research (Volume 364)

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353-358

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https://doi.org/10.4028/www.scientific.net/AMR.364.353

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Online since:

October 2011

Authors:

Yin Chew Ker, Abu Bakar Mohamad

Keywords:

Barium Nickel Titanium Oxide, Quaternary Metal Oxide, Spherical, Two-Step Sol-Gel Method

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