Preparation of Nano-Sized Tin Oxide by Polymer-Network Method

Shu Dong Geng; Fu Sheng Zhang; Yu Zhang; Lian Fa Chen; Wei Wang

doi:10.4028/www.scientific.net/AMR.391-392.789

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Preparation and Characterization of Fe₃₆Co₃₆B₂₀Si₄Nb₄ Nanocrystalline/Amorphous Matrix Composite
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A Comparative Study on Co-Sorption of Zn(II) and As(V) by Mixed Fe/Al-PILCs Prepared at Different Calcination Temperatures
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Preparation of Nano-Sized Tin Oxide by Polymer-Network Method
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A Thermo-Sensitive Laser Imaging Composition Derived from a Modified Phenolic Resin
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Effect of Amount on Expansion Property of MgO-Type Expansive Agent Used in Cement-Based Materials
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Mechanical Strength and Resistance to Ultraviolet Radiation of Repairing Mortars Based on Epoxy Resin
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Preparation of Nano-Sized Tin Oxide by Polymer-Network Method

Abstract:

SnO₂ has been widely used in the industry, and is important materials in the fields of electron, ceramics and chemistry. SnCl₄ was employed as raw material, acrylamide and N,N’-methylenediacrylamide were used as monomer and lattice reagent, respectively. In present work, SnO₂ nano-sized powder was prepared by the polymer-network method. The precursor was characterized using DTA-TG. The phase structure and particle size of the powder was determined by XRD and TEM, respectively. The results indicated that the SnO₂ powder with particle diameter size smaller than 50nm was obtained when the ratio of monomer and lattice reagent was 5:1, and the sintering temperature was 500 °C. Moreover, the distribution of powder particles was uniform and the specific surface area was big.