Preparation, Spectral Characterization and Crystal Structure 2-Acetyl-2'-Methoxylacetanilide

Li Hua Wang

doi:10.4028/www.scientific.net/AMR.396-398.1232

Paper Titles

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The Analysis of Mutual Authentication between Finite Element Analysis and Qi Erxi Answer
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Preparation, Spectral Characterization and Crystal Structure 2-Acetyl-2'-Methoxylacetanilide
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Present Status of Research and Application of Chemical Combination Flooding Technique and its Future
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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 396-398Preparation, Spectral Characterization and Crystal...

Preparation, Spectral Characterization and Crystal Structure 2-Acetyl-2'-Methoxylacetanilide

Abstract:

2-Acetyl-2'-methoxylacetanilide has been synthesized by the reaction of 2-methoxylaniline and ethyl acetoacetate in toluene solution. The compound was characterized by MS, Infrared spectrum, 1HNMR and X-ray single crystal diffraction analysis. The results show that the compound is target product. The crystal data for 2-acetyl-2'-methoxylacetanilide: monoclinic, space group P2(1)/c, Mr= 207.22, De = 1.309 g/cm3, F (000) = 440, R = 0.0826 and wR = 0.1822. The complex forms layered structure through ••• stacking interaction.