Synthesis and Characterization of Novel Poly (aryl ether sulfone ketone) S Containing M-Sulfonylbenzonyl Linkage in the Main Chains

Feng Ding; Da Zhi Wang; Shao Yin Zhang; Tian Xing Liu

doi:10.4028/www.scientific.net/AMR.396-398.1518

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 396-398Synthesis and Characterization of Novel Poly (aryl...

Synthesis and Characterization of Novel Poly (aryl ether sulfone ketone) S Containing M-Sulfonylbenzonyl Linkage in the Main Chains

Abstract:

A low expense chloro-monomer, 1-(4'-chloro-1-benzoyl)-3-(4'-1-choro-benzene sulfonyl)-benzene(CBCBSB), was synthesized by the Friedel-Crafts reaction of m-chlorosu1fonyl benzoyl chloride with chlorobenzene. A novel poly (aryl ether sulfone ketone)s (PAESK) containing m-sulfonylbenzoyl linkages in the main chains were prepared by copolycondensation of CBCBSB with hydroquinone in N, N-Dimethylacetamide (DMAc). The structure of PAESK was confirmed by FT-IR, 1H-NMR and characterized by XRD. thermogravimetry (TG) and Differential Scanning Calorimeter (DSC) were carried out to demonstrate its good melt processability. The polymer exhibited the better solubility in chloroform, N-methyl-2-pyrrlidone(NMP), dimethylacetamide(DMAC), dimethylformamide (DMF) and dimethylsulfoxide (DMSO) and excellent mechanical performance.

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Advanced Materials Research (Volumes 396-398)

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1518-1522

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.396-398.1518

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Online since:

November 2011

Authors:

Feng Ding, Da Zhi Wang, Shao Yin Zhang, Tian Xing Liu

Keywords:

1-(P-Chlorobenzoyl)-3-(P-Chloro-Benzenesul Fonyl) Benzene, Poly(Aryl Ether Sulfone Ketone), Thermal and Mechanical Properties

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