Analysis of Measuring Time for Au Nanoparticle Size Measurement by Photon Cross Correlation Spectroscopy

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Abstract:

It introduced the basic principle of measuring the size of nanoparticles by the method of Photon Cross-Correlation spectroscopy (PCCS). The measuring time for Au particle size measurement at different concentration using PCCS was studied. We measured gold particles with an average diameter of 24.5 nm at different concentration and different measuring times by PCCS. The measuring results demonstrate that for the same measuring time, the higher the concentration is, the smaller the standard deviation of repeated measurements is; for suspension of the same concentration, the longer the measuring time is, the smaller the standard deviation of repeated measurements is. It fitted the relationship between the standard deviation of measuring results and the measuring time at difference concentration. For the needed measuring accuracy, we can get the measuring time for some concentration according to the curve fitting.

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Advanced Materials Research (Volumes 403-408)

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1083-1088

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November 2011

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] Michael Kaszuba, The measurement of nanoparticles using photon correlation spectroscopy and avalanche photo diodes, Journal of Nanoparticle Research, vol. 1, 1999, pp.405-409.

Google Scholar

[2] Food R, Jakeman E, Oliver C, et al., Determination of diffusion coefficients of haemocyanin at low concentration by intensity fluctuation spectroscopy of scattered laser light, Nature, vol. 227, Jul. 1970, pp.242-245.

DOI: 10.1038/227242a0

Google Scholar

[3] Theodore Provder, Challenges in particle size distribution measurement past,present and for the 21st century, Progress in Organic Coalings(S0300-9440), vol. 32, 1997, pp.143-153.

DOI: 10.1016/s0300-9440(97)00043-x

Google Scholar

[4] Zetasizer Nano application note MRK1136-01, Effect of angle on resolving particle size mixture using dynamic light scatttering, Malvern Instruments, Ltd. (2008).

Google Scholar

[5] Schatzel, K. J. Mod. Optics, Vol. 38, 1991, p.1849.

Google Scholar

[6] Wiese, H., Horn, D., J. Chem. Phys. 1991, vol. 94, pp.6429-6443.

Google Scholar

[7] Dipl. Chem. Wolfgang Lammle, Sympate GmbH, Clausthal, Particle size and stability analysis in turbid suspensions and emulsions with Photon Cross Correlation Spectroscopy, unpublished.

Google Scholar

[8] W. Lammle, Nanometre particle sizing and stability measurment using a table-top PCCS system, LabPlus international, Mar. 2005, pp.19-24.

Google Scholar

[9] Koppel D E., Analysis of macromolecular polydispersity in intensity correlation spectroscopy: the method of cumulants, The Journal of Chemical Physics, vol. 57, num. 11, Dec. 1972, pp.4815-4820.

DOI: 10.1063/1.1678153

Google Scholar

[10] Provencher S W., A constrained regularization method for inverting date represented by linear algebraic or integral equations, Computer Physics Communication, vol. 27, 1982, pp.213-227.

DOI: 10.1016/0010-4655(82)90173-4

Google Scholar

[11] Dahneke B E, Wiley, Measurement of suspended particle by Quasi-Elastic Light Scattering, Journal of Clloid and Interface Science, vol. 98, Issue 2, Apr. 1984, pp.593-594.

DOI: 10.1016/s0021-9797(84)80085-5

Google Scholar

[12] Lan D. Morrison, E. F. Grabowski, C. A. Herb., Improved techniques for particle size determination by quasi-elastic light scattering, Langmuir, vol. 1, 1985, pp.496-501.

DOI: 10.1021/la00064a016

Google Scholar